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GCMS analysis results for sample AE10242, May 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AE10242 conducted on May 28, 2002, including surrogate recovery data.

NYC-WTC_000024804–000024812

Folder label: “GCMS X 5/14/02 A 5/17/02

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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\MSDCHEM\1\DATA\020509\10242.D Vial: 20 Acq On : 10 May 2002 5:24 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Smoothing : ON Filtering: 5 Sampling : 1 Min Area: 0.7 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 6.152 516 523 553 rBV 515190 1053481 21.58% 4.001% 2 11.376 1398 1412 1433 rBV 1336886 3449553 70.65% 13.102% 3 16.534 2273 2290 2306 rBV 1633440 4369797 89.50% 16.597% 4 24.461 3620 3639 3655 rBV2 1620035 4551402 93.22% 17.287% 5 24.607 3655 3664 3673 rVB5 17292 50460 1.03% 0.192%

6 27.533 4149 4162 4177 rBV4 196298 546680 11.20% 2.076% 7 31.088 4757 4767 4781 rVB4 12722 44568 0.91% 0.169% 8 31.717 4855 4874 4900 rBV2 1637358 4882547 100.00% 18.544% 9 31.952 4905 4914 4924 rVB4 13830 40987 0.84% 0.156% 10 39.931 6260 6272 6291 rBV2 2167093 4255748 87.16% 16.164%

11 43.151 6809 6820 6844 rBV2 1513881 3083837 63.16% 11.713%

Sum of corrected areas: 26329060

10242.D SCAN020507.M Tue May 14 14:25:43 2002 Page 1

NYC-WTC_000024806

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NYC-WTC_000024806Source: NYC Law Department, mirrored locally

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GCMS sample preparation log, May 2002 · Box DEP Box 18

NYC-WTC_000024427

Record of sample preparation parameters including drip rates and volumes for GCMS analysis conducted in mid-May 2002.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993

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