Reference document describing Method 509 procedures for laboratory analysis, dated February 14, 1992.
NYC-WTC_000024748–000024757Folder label: “GCMS X 5/14/02 A 5/17/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File : C:\MSDCHEM\1\DATA\020516\0514LB.D Vial: 5 Acq On : 16 May 2002 1:19 pm Operator: Nefliu Sample : 05/14 lab blk Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Time: May 17 10:34:33 2002 Quant Results File: SCAN020507.RE Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Thu May 16 14:49:15 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1
Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.38 152 313829 40.00 ug/1 -0.01 10) Naphthalene-d8 16.53 136 1195146 40.00 ug/1 -0.04 17) Acenaphthene-diO 24.46 164 635570 40.00 ug/1 -0.02 30) Phenanthrene-diO 31.72 188 1090325 40.00 ug/1 -0.02 38) Chrysene-dl2 39.93 240 866788 40.00 ug/1 -0.05 44) Perylene-dl2 43.15 264 504842 40.00 ug/1 -0.03
System Monitoring Compounds 27) TCMX 27.55 207 159474 31.41 ug/1 -0.02 Spiked Amount 40.000 Recovery 78.53% Target Compounds Qvalue
(#) = qualifier out of range (m) = manual integration (+) = signals summed 0514LB.D SCAN020507.M Fri May 17 10:35:58 2002 Page 1
NYC-WTC_000024749
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NYC-WTC_000024427
Record of sample preparation parameters including drip rates and volumes for GCMS analysis conducted in mid-May 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024534
Laboratory report showing blank test results for GCMS analysis of sample AE11282 conducted between May 13 and May 16, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025499
Laboratory report showing non-detect levels for 15 volatile organic compounds in a GCMS method blank processed on May 17-21, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022495
Technical log detailing gas chromatography mass spectrometry method parameters and calibration settings from May 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024629
Laboratory report showing blank test results for GCMS analysis of sample AE11157 conducted between May 13 and May 16, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025568
GCMS analysis report for sample AE11567 showing unknown compounds and surrogate recovery data from May 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024706
Laboratory report documenting GCMS analysis of sample AE11281 conducted on May 22, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024652
GCMS analysis for sample AE11157 identifying other unknown compounds with a 2,4-DDD surrogate recovery of 91%, completed May 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024907
Laboratory report documenting GCMS analysis of sample AE10247 conducted on May 28, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024851
GCMS analysis results for sample AE10245 conducted May 28, 2002, showing unknown compounds and 2,4-DDD surrogate recovery at 86 percent.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046117
Laboratory report showing GCMS blank results for volatile organic compounds from sample AE10068 dated May 7-13, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048602
Laboratory blank analysis results confirming absence of contamination in GCMS testing for volatile organic compounds.
1 shared topics · similarity 0.992
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NYC-WTC_000024743
Department of Environmental Protection administrative record sheet for World Trade Center site activities dated May 2002.
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NYC-WTC_000024744
Index or cover page for the GCMS document series covering samples from May 14 to May 17, 2002.
Filed in the same folder
NYC-WTC_000024758
Laboratory report of a GCMS blank run for sample AE10241 conducted between May 14 and May 16, 2002.
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NYC-WTC_000024762
Laboratory report of GCMS calibration data for sample AE10241 conducted between May 14 and May 16, 2002.
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NYC-WTC_000024770
Laboratory report of GCMS analysis for sample AE10241 conducted on May 28, 2002.
Filed in the same folder