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GCMS method parameters and calibration data, May 2002

Machine-extracted title · confidence 95%

Technical log detailing gas chromatography mass spectrometry method parameters and calibration settings from May 2002.

NYC-WTC_000022495–000022503

Folder label: “GCMS X 5/17/12 A 5/21/02

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Scanned page image, NYC-WTC_000022496
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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File : C:\MSDCHEM\1\DATA\020521\0517LB1.D Vial: 3 Acq On : 21 May 2002 10:15 am Operator: Nefliu Sample : 05/17 lab blk kea Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Time: May 24 09:09:36 2002 Quant Results File: SCAN020521.RE Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Tue May 21 08:15:50 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.37 152 410782 40.00 ug/1 -0.02 10) Naphthalene-d8 16.53 136 1563198 40.00 ug/1 -0.04 17) Acenaphthene-dl0 24.46 164 832934 40.00 ug/1 -0.02 30) Phenanthrene-dl0 31.72 188 1417094 40.00 ug/1 -0.02 38) Chrysene-dl2 39.93 240 1033006 40.00 ug/1 -0.05 44) Perylene-dl2 43.15 264 596898 40.00 ug/1 -0.03 System Monitoring Compounds 27) TCMX 27.56 207 227176 34.00 ug/1 -0.04 Spiked Amount 40.000 Recovery 85.00% Target Compounds Qvalue

(#) = qualifier out of range (m) = manual integration (+) = signals summed 0517LB1.D SCAN020521.M Fri May 24 09:13:12 2002 Page 1

NYC-WTC_000022496

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NYC-WTC_000022496Source: NYC Law Department, mirrored locally

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