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GCMS blank results for sample AE11282, May 2002

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Laboratory report showing blank test results for GCMS analysis of sample AE11282 conducted between May 13 and May 16, 2002.

NYC-WTC_000024534–000024542

Folder label: “GCMS X 5/13/02 A 5/16/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\1\DATA\020516\0513LB.D Vial: 4 Acq On : 16 May 2002 12:20 pm Operator: Nefliu Sample : 05/13 lab blk Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Time: May 17 10:03:48 2002 Quant Results File: SCAN020507.RE

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Thu May 16 14:49:15 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.38 152 347246 40.00 ug/1 -0.01 10) Naphthalene-d8 16.53 136 1310071 40.00 ug/1 -0.04 17) Acenaphthene-diO 24.46 164 705574 40.00 ug/1 -0.02 30) Phenanthrene-diO 31.72 188 1217713 40.00 ug/1 -0.02 38) Chrysene-dl2 39.93 240 997140 40.00 ug/1 -0.05 44) Perylene-dl2 43.15 264 588462 40.00 ug/1 -0.03

System Monitoring Compounds 27) TCMX 27.56 207 187070 33.19 ug/1 -0.02 Spiked Amount 40,000 Recovery 82.97%

Target Compounds Qvalue 43) Bis(2-ethylhexyl)phthalate 40.52 149 65155 3.05 ug/1 95

(#) = qualifier out of range (m) = manual integration (+) = signals summed 0513LB.D SCAN020507 .M Fri May 17 10:29:53 2002 Page 1

NYC-WTC_000024535

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NYC-WTC_000024535Source: NYC Law Department, mirrored locally

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GCMS sample preparation log, May 2002 · Box DEP Box 18

NYC-WTC_000024427

Record of sample preparation parameters including drip rates and volumes for GCMS analysis conducted in mid-May 2002.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995

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