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GCMS blank results for sample AE11157, May 2002

Machine-extracted title · confidence 100%

Laboratory report showing blank test results for GCMS analysis of sample AE11157 conducted between May 13 and May 16, 2002.

NYC-WTC_000024629–000024639

Folder label: “GCMS X 5/13/02 A 5/15/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File : C:\MSDCHEM\1\DATA\020515\0513LB1.D Vial: 3 Acq On : 15 May 2002 1:48 pm Operator: Nefliu Sample : 05/13 lab blk Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Time: May 15 15:22:42 2002 Quant Results File: SCAN020507.RE Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Wed May 15 15:22:39 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1 Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.37 152 398205 40.00 ug/1 -0.02 10) Naphthalene-d8 16.53 136 1483681 40.00 ug/1 -0.04 17) Acenaphthene-diO 24.46 164 798046 40.00 ug/1 -0.02 30) Phenanthrene-diO 31.72 188 1345060 40.00 ug/1 -0.02 38) Chrysene-dl2 39.93 240 971431 40.00 ug/1 -0.05 44) Perylene-dl2 43.15 264 646629 40.00 ug/1 -0.03

System Monitoring Compounds 27) TCMX 27.55 207 222646 34.92 ug/1 -0.02 Spiked Amount 40.000 Recovery 87.30% Target Compounds Qvalue 43) Bis(2-ethylhexyl)phthalate 40.52 149 33954 1.63 ug/1 95

(#) = qualifier out of range (m) = manual integration (+) = signals summed 0513LB1.D SCAN020507.M Thu May 16 14:42:59 2002 Page 1

NYC-WTC_000024630

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NYC-WTC_000024630Source: NYC Law Department, mirrored locally

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GCMS sample preparation log, May 2002 · Box DEP Box 18

NYC-WTC_000024427

Record of sample preparation parameters including drip rates and volumes for GCMS analysis conducted in mid-May 2002.

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