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GCMS analysis results for sample AE11281, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE11281 conducted on May 22, 2002, including surrogate recovery data.

NYC-WTC_000024706–000024718

Folder label: “GCMS X 5/13/02 A 5/15/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File : C:\MSDCHEM\l\DATA\020515\11281.D Vial: 15 Acq On : 16 May 2002 1:38 am Operator: Nefliu Sample : sample Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Time: May 16 09:59:35 2002 Quant Results File: SCAN020507 .RE Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Wed May 15 15:22:39 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1 Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.38 152 447925 40.00 ug/1 -0.01 10) Naphthalene-d8 16.53 136 1681655 40.00 ug/1 -0.04 17) Acenaphthene-diO 24.46 164 906528 40.00 ug/1 -0.02 30) Phenanthrene-diO 31.72 188 1527886 40.00 ug/1 -0.02 38) Chrysene-dl2 39.93 240 1219327 40.00 ug/1 -0.05 44) Perylene-dl2 43.15 264 725431 40.00 ug/1 -0.03

System Monitoring Compounds 27) TCMX 27.56 207 260795 36.01 ug/1 -0.02 Spiked Amount 40.000 Recovery 90.03% Target Compounds Qvalue 43) Bis(2-ethylhexyl)phthalate 40.52 149 42028 1.61 ug/1 97

(#) = qualifier out of range (m) = manual integration (+) = signals summed 11281.D SCAN020507.M Thu May 16 10:00:47 2002 Page 1

NYC-WTC_000024708

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NYC-WTC_000024708Source: NYC Law Department, mirrored locally

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