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GCMS analysis results, sample AE10987, May 2002

Machine-extracted title · confidence 80%

Gas chromatography-mass spectrometry analysis of sample AE10987 completed May 22, 2002, showing unknown compounds and surrogate recovery at 89%.

NYC-WTC_000024463–000024471

Folder label: “GCMS X 5/13/02 A 5/16/02

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Scanned page image, NYC-WTC_000024465
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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File : C:\MSDCHEM\1\DATA\020515\10987.D Vial: 17 Acq On : 16 May 2002 3:36 am Operator: Nefliu Sample : sample Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Time: May 16 08:39:50 2002 Quant Results File: SCAN020507.RE Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Wed May 15 15:22:39 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1 Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.37 152 453980 40.00 ug/1 -0.02 10) Naphthalene-d8 16.53 136 1719996 40.00 ug/1 -0.04 17) Acenaphthene-diO 24.45 164 926710 40.00 ug/1 -0.02 30) Phenanthrene-dlO 31.72 188 1571637 40.00 ug/1 -0.02 38) Chrysene-dl2 39.93 240 1268519 40.00 ug/1 -0.05 44) Perylene-dl2 43.15 264 757299 40.00 ug/1 -0.03 System Monitoring Compounds 27) TCMX 27.55 207 262356 35.44 ug/1 -0.02 Spiked Amount 40.000 Recovery 88.60% Target Compounds Qvalue 43) Bis(2-ethylhexyl)phthalate 40.52 149 148340 5.46 ug/1 95

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(#) = qualifier out of range (m) = manual integration (+) = signals summed 10987 .D SCAN020507.M Thu May 16 09:24:35 2002 Page 1

NYC-WTC_000024465

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NYC-WTC_000024465Source: NYC Law Department, mirrored locally

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