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GCMS analysis results for sample AE11152, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE11152 conducted on May 22, 2002, including surrogate recovery data.

NYC-WTC_000024472–000024483

Folder label: “GCMS X 5/13/02 A 5/16/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File : C:\MSDCHEM\l\DATA\020515\11152.D Vial: 18 Acq On : 16 May 2002 4:35 am Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Time: May 16 08:39:59 2002 Quant Results File: SCAN020507.RE Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Wed May 15 15:22:39 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.38 152 466648 40.00 ug/1 -0.01 10) Naphthalene-d8 16.53 136 1749370 40.00 ug/1 -0.04 17) Acenaphthene-diO 24.46 164 948810 40.00 ug/1 -0.02 30) Phenanthrene-diO 31.72 188 1613098 40.00 ug/1 -0.02 38) Chrysene-dl2 39.93 240 1311109 40.00 ug/1 -0.05 44) Perylene-dl2 43.15 264 809633 40.00 ug/1 -0.03

System Monitoring Compounds 27) TCMX 27.55 207 266810 35.20 ug/1 -0.02 Spiked Amount 40.000 Recovery 88.00% Target Compounds Qvalue 43) Bis(2-ethylhexyl)phthalate 40.52 149 150639 5.36 ug/1 95

(#) = qualifier out of range (m) = manual integration (+) = signals summed 11152.D SCAN020507.M Thu May 16 09:28:25 2002 Page 1

NYC-WTC_000024474

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NYC-WTC_000024474Source: NYC Law Department, mirrored locally

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