GCMS analysis results for sample AE11155, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020515\11155.D Vial: 21 Acq On : 16 May 2002 7:34 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 12 1,3-Bis(dimethyl-n-pentylsi... Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

10.64 0.62 ug/1 46423 1,4-Dichlorobenzene-d4 11.38

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,3-Bis (dimethyl-n-pentylsilyl) p. . . 298 C17H38Si2 1000214-94-5 12 2 l-Trimethylsily-2-(dimethyl-n-pe... 228 C12H28Si2 1000214-91-7 10 3 4,4,5,5-Tetramethyl-2-oxazolidinone 143 C7H13N02 052856-03-8 9 4 Silane,/ethyldimethyl- 88 C4H12Si 000758-21-4 9 Abundance Scan 1287 (10.641 min): 11155.D (-1281) (-) m/z 43.05 100.00% 43

59 MAU/ 5000 73 104 10.40 10.60 10.80 11.00

z—> IIT 20 44044444487— -- 307 60 80 100 120 140 160 180 200 220 240 260 280 300 193207 i ■ ‘ 1 ■ i ■ 1 ' 1 i ■ ■ ' ■ i ' ■ ■ ■ i ■ ' m/ z 59.00 52.29% Abundance #19895:1,3-Bis(dimethyl-n-pentylsilyl)propene 59

129 In A । A । aka , ) ..A 5000’ 73 10.40 10,60 10.80 11.00 m/z 73.10 27.40% 43 87 1= 228 11.... h ।. ll ■ q"'I. | TI ′ 120113, TI i i 1143 | 11T‘ 185 I I I ‘TI I . i . | r I . , | i .213 | , | , TTTf t > I . I i r. i 171u 283298I I I . niz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #19894:1-Trimethylsily-2-(dimethyl-n-pentylsilyl)ethene 59 1,1..A A A, 10.40 10,60 10.80 11,00 5000 73 129 m/ z 46.00 27.08%

43 158 143 । RR 99 111 11 Mhi 144 ■, iff, il al hi/ ■ ■ T|| ' ■ ' ■ i 1 ■ ■ ■ i 1 213 228 • ■ 1 I 1 1 1 1 I । 1 1 । I । 1 । ' I ' । 1 1 1 1 1 mlz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #19378:4,4,5,5-Tetramethyl-2-oxazolidinone 42 59 10.40 10,60 10.80 11.00 m/z 104.10 23.88%

5000 84 115 28 100 128 143 ‘ ' T' ' ‘ 1 I ' ■ ' ' I ■ i11 ■ ■ । ■ ■ ■ ■ ।1 ■ ■ ■ ।1111111111 I ' ’ ' 1 I 1 ' * I 1 1 1 1 I m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 10.40 10.60 10.80 11.00

11155.D SCAN020507.M Thu May 16 09:35:08 2002 Page 14

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