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GCMS chain of custody form, sample AE10986, May 2002

Machine-extracted title · confidence 100%

Chain of custody record for GCMS analysis of sample AE10986 on May 22, 2002, including surrogate compound data.

NYC-WTC_000024450–000024462

Folder label: “GCMS X 5/13/02 A 5/16/02

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Scanned page image, NYC-WTC_000024452
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document yuciltAtatAOi KCpOL L 1 Keviewed)

Data File : C:\MSDCHEM\1\DATA\020515\10986.D Vial: 16 Acq On : 16 May 2002 2:37 am Operator: Nefliu Sample : sample Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Time: May 16 08:39:41 2002 Quant Results File: SCAN020507.RE

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Wed May 15 15:22:39 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.38 152 418695 40.00 ug/1 -0.01 10) Naphthalene-d8 16.53 136 1585517 40.00 ug/1 -0.04 17) Acenaphthene-diO 24.45 164 829755 40.00 ug/1 -0.02 30) Phenanthrene-diO 31.71 188 1408175 40.00 ug/1 -0.03 38) Chrysene-dl 2 39.93 240 1136828 40.00 ug/1 -0.05 44) Perylene-dl2 43.15 264 682480 40.00 ug/1 -0.03

System Monitoring Compounds 27) TCMX 27.55 207 229116 34.57 ug/1 -0.02 Spiked Amount 40.000 Recovery 86.42%

Target Compounds Qvalue 3 9) Pyrene 36.66 202 82 0.00 ug/1 # 58 43) Bis(2-ethylhexyl )phthalate 40.52 149 131406 5.40 ug/1 93

(#) = qualifier out of range (m) = manual integration (+) = signals summed 10986.D SCAN020507.M Thu May 16 09:22:47 2002 Page 1

NYC-WTC_000024452

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NYC-WTC_000024452Source: NYC Law Department, mirrored locally

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