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GCMS analysis results for sample AE10704, May 20 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry report for sample AE10704 showing detection of unknown compounds and surrogate recovery.

NYC-WTC_000045793–000045810

Folder label: “GCMS X 5/3/02 A 5/13/02

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NYC 9/11 Public Portal Document 01 reviewed)

Data File : C:\MSDCHEM\l\DATA\020513\10704.D Vial: 15 Acq On : 14 May 2002 2:23 am Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Time: May 15 08:59:28 2002 Quant Results File: SCAN020507 .RE Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Thu May 09 09:21:01 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.38 152 554984 40.00 ug/1 -0.01 10) Naphthalene-d8 16.54 136 2091779 40.00 ug/1 -0.03 17) Acenaphthene-diO 24.47 164 1123816 40.00 ug/1 -0.01 30) Phenanthrene-diO 31.72 188 1905232 40.00 ug/1 -0.02 38) Chrysene-dl2 39.94 240 1399208 40.00 ug/1 -0.05 44) Perylene-dl2 43.16 264 864902 40.00 ug/1 -0.02

System Monitoring Compounds 27) TCMX 27.54 207 67204 7.49 ug/1 -0.04 Spiked Amount 10.000 Recovery = 74.90% Target Compounds Qvalue 43) Bis(2-ethylhexyl)phthalate 40.52 149 15063 0.50 ug/1 94

(#) = qualifier out of range (m) = manual integration (+) = signals summed 10704.D SCAN020507.M Wed May 15 09:01:03 2002 Page 1

NYC-WTC_000045795

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NYC-WTC_000045795Source: NYC Law Department, mirrored locally

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