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GCMS sample analysis results for AE10698, May 20 2002

Machine-extracted title · confidence 100%

Laboratory report detailing GC/MS analysis of sample AE10698 including surrogate recovery data in May 2002.

NYC-WTC_000045707–000045720

Folder label: “GCMS X 5/3/02 A 5/13/02

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Scanned page image, NYC-WTC_000045709
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NYC 9/11 Public Portal Document

-Data File : C:\MSDCHEM\l\DATA\020513\10698.D Vial: 9 Acq On : 13 May 2002 8:26 pm Operator: Nefliu Sample : sample Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Time: May 15 08:32:23 2002 Quant Results File: SCAN020507.RE

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Thu May 09 09:21:01 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.38 152 407316 40.00 ug/1 -0.01 10) Naphthalene-d8 16.53 136 1523468 40.00 ug/1 -0.04 17) Acenaphthene-diO 24.45 164 812503 40.00 ug/1 -0.02 30) Phenanthrene-diO 31.72 188 1403057 40.00 ug/1 -0.02 38) Chrysene-dl2 39.93 240 1144730 40.00 ug/1 -0.05 44) Perylene-dl2 43.15 264 715394 40.00 ug/1 -0.03

System Monitoring Compounds 2 7) TCMX 27.54 207 46910 7.23 ug/1 -0.04 Spiked Amount 10.000 Recovery = 72.30%

Target Compounds Qvalue 43) Bis(2-ethylhexyl)phthalate 40.52 149 4515 0.18 ug/1 82

(#) = qualifier out of range (m) = manual integration (+) = signals summed 10698.D SCAN020507.M Wed May 15 08:33:33 2002 Page 1

NYC-WTC_000045709

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NYC-WTC_000045709Source: NYC Law Department, mirrored locally

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