Gas chromatography-mass spectrometry analysis of sample AE10895 with 91% surrogate recovery for 2,4-DDD, conducted May 21, 2002.
NYC-WTC_000024070–000024082Folder label: “GCMS X 5/10/02 A 5/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document yuanttatlon Report (QT Reviewed)
Data File : C:\MSDCHEM\l\DATA\051602\10895.D Vial: 8 Acq On : 16 May 2002 8:14 pm Operator: Mclean Sample : 5/10 eh Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: May 17 09:44:53 2002 Quant Results File: 050102.RES
Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Mon May 13 11:40:29 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 9.93 152 4486162 40.00 ug/L 0.00 10) Napthalene-d8 13.43 136 17753956 40.00 ug/L 0.00 17) Acenapthalene-dlO 18.57 164 9567790 40.00 ug/L 0.00 29) Phenanthranene-dlO 22.95 188 13381965 40.00 ug/L 0.00 37) Chrysene-dl2 30.80 240 8911563 40.00 ug/L 0.00 43) Perylene-dl2 34.70 264 5066834 40.00 ug/L 0.00
System Monitoring Compounds 27) TCMX 20.54 209 2125217 36.59 ug/L 0.00 Spiked Amount 40.000 Recovery 91.48%
Target Compounds Qvalue 2) n-nitros-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2‘oxybis(1-Chloropropane 0.00 45 0 N.D. 8) N-nitroso-di-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy) methan 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Napthalene 0.00 128 0 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) 2-Chloronaphthalene 0.00 162 0 N.D. 19) Dimethylphthalate 0.00 163 0 N.D. 20) 2,6-Dinitrotoluene 0.00 165 0 N.D. 21) Acenapthylene 0.00 152 0 N.D. 22) Acenapthalene 0.00 153 0 N.D. 23) 2,4-Dinitrotoluene 0.00 165 0 N.D. 24) Diethylphthalate 0.00 149 0 N.D. 25) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 26) Fluorene 0.00 166 0 N.D. 28) Azobenzene 20.54 77 36821 N.D. 30) Nnitrosodiphenylamine 20.54 169 40232 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0 .-0 0 284 0 N.D. 3 3) Phenanthrene 0.00 178 0 N.D. 34) Anthracene 0.00 178 0 N.D. 35) Di-n-butylphthalate 0.00 149 0 N.D.
(#) = qualifier out of range (m) = manual integration 10895.D 050102.M Fri May 17 15:03:28 2002 Page 1
NYC-WTC_000024072
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NYC-WTC_000022916
Laboratory report documenting GCMS analysis of environmental sample AE09568 conducted on May 15, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024153
Document noting low recovery in GCMS scan of sample AE10205 and subsequent re-extraction yielding 85% recovery.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023887
Laboratory report showing GC/MS analysis of sample AE10980 with surrogate recovery data for 2,4-DDD.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023502
Laboratory report showing GC/MS analysis results for sample AE10816 including surrogate recovery data on May 14, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022938
Laboratory report documenting GCMS analysis of environmental sample AE09569 conducted on May 15, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023487
Laboratory report showing GC/MS analysis results for sample AE10164 including surrogate recovery data on May 14, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023531
Laboratory report page showing GC/MS analysis for sample AE10850 including surrogate recovery data on May 14, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023439
Laboratory report showing GC/MS analysis results for sample AE10137 including surrogate recovery data on May 14, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024113
Laboratory report detailing GCMS analysis of sample AE10898 conducted on May 21, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022795
GCMS analytical report for environmental sample AE09151 including surrogate compound data from May 15, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024083
Laboratory report detailing GCMS analysis of sample AE10896 conducted on May 21, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025332
Fragmented document containing GC/MS data from May 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000024038
Department of Environmental Protection administrative record sheet for World Trade Center site activities dated May 2002.
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NYC-WTC_000024039
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Laboratory report showing non-detectable levels of nitrosamines and other contaminants in blank sample AE10895.
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Laboratory report showing calibration data for volatile organic compounds in sample AE10895 analysis.
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Laboratory report showing reference standard analysis results for nitrosamines and other compounds in sample AE10895.
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