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Laboratory report showing GC/MS analysis of sample AE10981 with surrogate recovery data for 2,4-DDD.
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machine-extracted · confidence unavailable · Check page ↗Document / 22 pages
GCMS analysis results, sample AE09155, May 2002
Machine-extracted title · confidence 100%GCMS analytical report for environmental sample AE09155 including surrogate compound data from May 15, 2002.
NYC-WTC_000022857–000022878Folder label: “GCMS X 5/8/02 A 5/10/02”
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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)
Data File : C:\MSDCHEM\1\DATA\050902\9155.D Vial: 20 Acq On : 10 May 2002 7:36 am Operator: Mclean Sample : 5/8 eh Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: May 13 11:41:04 2002 iQuant Results File: 050102.RES j
Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Mon May 13 11:40:29 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 9.93 152 5478603 40.00 ug/L 0.00 10) Napthalene-d8 13.43 136 21394510 40.00 ug/L 0.00 17) Acenapthalene-dlO 18.57 164 11649863 40.00 ug/L 0.00 29) Phenanthranene-dlO 22.95 188 16772912 40.00 ug/L 0.00 37) Chrysene-dl 2 30.80 240 10835955 40.00 ug/L 0.00 43) Perylene-dl2 34.70 264 5526591 40.00 ug/L -0.01
System Monitoring Compounds 27) TCMX 20.54 209 2077414 :29.37 ug/L 0.00 Spiked Amount 40.000 Recovery 73.43%
Target Compounds Qvalue 2) n-nitros-dimethyl amine 0.00 74 0 N.D. d 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'oxybis(1-Chloropropane 0.00 45 0 N.D. 8) N-nitroso-di-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy) methan 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Napthalene 0.00 128 0 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) 2-Chloronaphthalene 0.00 162 0 N.D. 19) Dimethylphthalate 0.00 163 0 N.D. 20) 2,6-Dinitrotoluene 0.00 165 0 N.D. 21) Acenapthylene 0.00 152 0 N.D. 22) Acenapthalene 0.00 153 0 N.D. 23) 2,4-Dinitrotoluene 0.00 165 0 N.D. 24) Diethylphthalate 0.00 149 0 N.D. 25) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 26) Fluorene 0.00 166 0 N.D. 28) Azobenzene 20.54 77 34478 N.D. 30) Nnitrosodiphenylamine 20.54 169 38816 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 0.00 178 0 N.D. 3 4) Anthracene 0.00 178 0 N.D. 35) Di-n-butylphthalate 25.09 149 15318 N.D.
(#) = qualifier out of range (m) = manual integration 9155.D 050102.M Mon May 13 11:41:36 2002 Page 1
NYC-WTC_000022859
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