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GCMS analysis with surrogate recovery, sample AE10895, May 2002

Machine-extracted title · confidence 80%

Gas chromatography-mass spectrometry analysis of sample AE10895 with 91% surrogate recovery for 2,4-DDD, conducted May 21, 2002.

NYC-WTC_000024070–000024082

Folder label: “GCMS X 5/10/02 A 5/16/02

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Scanned page image, NYC-WTC_000024073
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NYC 9/11 Public Portal Document quantitation Report (QT Reviewed) Data File : C:\MSDCHEM\1\DATA\051602\10895.D Vial: 8 Acq On : 16 May 2002 8:14 pm Operator: Mclean Sample : 5/10 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: May 17 09:44:53 2002 Quant Results File: 050102.RES Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Mon May 13 11:40:29 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Compound R.T. Qlon Response Cone Unit Qvalue 36) Fluoroanthene 0.00 202 0 N.D. 38) Pyrene 0.00 202 0 N.D. 39) Butylbenzylphthalate 0.00 149 0 N.D. 40) Benzo(a)anthracene 30.80 228 19441 N.D. 41) Bis(2-ethylhexyl)phthalate 31.37 149 85034 0.39 ug/L 94 42) Chrysene 0.00 228 0 N.D. 44) Di-n-octylphthalate 0.00 149 0 N.D. 45) Benzo(b)fluoranthene 0.00 252 0 N.D. 46) Benzo(k)fluoranthene 0.00 252 0 N.D. 47) Benzo(a)pyrene 0.00 252 0 N.D. 48) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 49) Dibenz(a,h)anthracene 0.00 278 0 N.D. 50) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration (+) = signals summed 10895.D 050102.M Fri May 17 15:03:28 2002 Page 2

NYC-WTC_000024073

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NYC-WTC_000024073Source: NYC Law Department, mirrored locally

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