GC/MS results for unknown compounds and surrogates, sample AE10985, May

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Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\051402\10985.D Vial: 14 Acq On : 15 May 2002 12:06 am Operator: Mclean Sample : 5/10 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 5 Thiirane, methyl- Concentration Rank 15

R.T. EstConc Area Relative to ISTD R.T.

5.65 0.21 ug/L 169697 1,4-Dichlorobenzene-d4 9.93

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Thiirane, methyl- 74 C3H6S 001072-43-1 4/ 2 Allyl mercaptan 74 C3H6S 000870-23-5 A 3 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0/4 4 Acetonitrile, dichloro- 109 C2HC12N 003018-12-/ 4 Abundance Scan 437 (5.647 min): 10985.D (-424) (-) m/ z 74.10 100.00% 74

59 5000 35 50 88 5.40 5.60 5.80 6.00 01 1 ' । 1 1 ■ ' i ■ ■ ■ ■ i ■ ■ i ■ 1 11 ■ 1 । 1 1 1 ' । * ■ i 1 1 ' i ■ 1 ■ r i 1 ' ' ' i ' 1 ' ■ i m/Z 59.10 58.01% miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #115343: Thiirane, methyl- 41 74

5000 5.40 5.60 5.80 6.00 47 m/z 35.10 29.13% 27 22 , 01 ------- + 11,,53.59..88, 'I 1 1 1 > । । I 1 '' 1 I ' 1 1 ' I 1 1 1 1 I m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28161: Allyl mercaptan 41 74 fl

5.40 5.60 5.80 6.00 5000 m/z 39.10 28.76%

47 27 33 । 01 --- |l, 53 5% , 68,1 ——————— +' I 1 1 11 i 1 1 1 ' r1 mfe-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28338: Acetonitrile, dichloro- T"11n . 1*1 tTr T TTr ■ r1 74 5.40 5.60 5.80 6.00 m/z 76.00 26.82% 5000 82 47 35 — 12 26 , 108 m/z-> 0 1 1 I 1 1 1 1 I ' 1,1,1 10 20 ;30 40 Il 50 ....606211 70 80 1 1 1 1 ' 1 1 i 1 1 1 '' I 1 1 1 1 1 90 100 110 5.40 5.60 5.80 6.00

10985.D 050102.M Thu May 16 14:42:34 2002 Page 8

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