GCMS analysis results for sample AE11929, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\052302\11929.D Vial: 9 Acq On : 23 May 2002 4:29 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) • Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 1 Acetonitrile, dichloro- Concentration Rank 16

R.T. EstConc Area Relative to ISTD R.T.

3.54 0.23 ug/L 164069 1,4-Dichlorobenzene-d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 59 2 3,3-Dichloropropyne 108 C3H2C12 1000222-23-917 3 Allyl mercaptan 74 C3H6S 000870-23-5/ 9 4 Thiirane, methyl- 74 C3H6S 001072-43-1 9 Abundance Scan 78 (3.537 min): 11929.D (-73) (-) m/z 74.00 100.00% 74 82

... o... . 5000 48 38 55 3.20 3.40 3.60 3.80

mfe-> 0- mm H11 10 20 30 40 50 60 70 80 TLB t 88 1 i ' ‘

90 • i ■ ■ ‘ ■ i ■ ■ ‘ ■ i

100 110 m/z 82.00 74.10% Abundance #28338: Acetonitrile, dichloro- 74

5000 82 n4—iDh—."OMmmapotakru 3.20 3.40 3.60 3.80 47 m/z 76.10 36.45% 35 01 ——— 12 ,26,.. -—2— TIB . * ■ i • ‘ 108 ■ i ■ ■ ■ 1 l ■ ■ ■ ‘ i

n/z-> 10 201 30 40 50 60 70 80 90 100 110 Abundance #28312:3,3-Dichloropropyne 74 1 i ■ ■ ■ ■ i ■ i ■ • * • i 3.20 3.40 3.60 3.80 5000 m/z 48.00 30.42%

-n/z-> 01 1999—— 10 20 28 30 38

40 47 ,1,53.460 44 50 60 70 82 108 1 I 1 1 1 1 i ■ ■ ■ ■ i * • ■ ■ i ■ ■ ■ ■ i 80 90 100 110 MWMysa Abundance #28161: Allyl mercaptan ■ i ‘ ■ i ■ 1 ■ > । ■ ■ ■ ■ i ■ ' ■ 1 । 41 74 3.20 3.40 3.60 3.80 m/z 47.10 27.56% 5000

47 ’akup/. 27 33 । 0- 111 Ml-153.59.4 68, 1 — ■ । ‘ । ■ • ■ ■ । ■ ■ • ■ । । miz-> 10 20 30 40 50 60 70 80 90 100 110 3.20 3.40 3.60 3.80

11929.D 052202.M Wed May 29 09:49:29 2002 Page 4

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