GCMS analysis results for sample AE11384, May 22 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\051702\11383.D Vial: 10 Acq On : 17 May 2002 8:07 pm Operator: Mclean Sample : 5/15 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHQDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 1 Acetonitrile, dichloro- Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 3.63 0.31 ug/L 293485 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qu.

l Acetonitrile, - dichloro- 109 C2HC12N 003018-12-0 91 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 56 3 Allyl mercaptan 74 C3H6S 000870-23-5 25 4 Thiirane, methyl- 74 C3H6S 001072-43-1 5 Abundance Scan 93 (3.626 min): 11383. D (-88) (-) m/ z 74.00 100.00%] 74

82 5000 47 __________ i 1 1 35 3.20 3.40 3.60 3.80 4.00

m/z-> 0+ 1 i ' ■ ' ' i ' ‘ ‘ 1 i ' ' 1 1 I ' 10 20 30 40 ll 58 ------------ 50 60 70 I 80 ‘ i ‘ ‘ 90 ' i ' ' ' ■ i ' ‘ 100 110 ' I m/z 82.00 52.64%| Abundance #28338: Acetonitrile, dichloro- 74

5000 47 82 A 3.20 3.40 3.60 3.80 4.00 m/z 76.00 32.33% 35 12 26 | |H . 108 Of 1 > [ I I t I I I I ' I ’ I I I I I I I I PT Hi................. ' •fil । ■ । 1 1 ' . । । > TtI । . . . । n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #115342: Acetonitrile, dichloro- 74 35 ........ . 3.20 3.40 3.60 3.80 4.00 5000 82 m/z 47.00 30.48% 47

miz-> 01

Abundance 1I**1IIIII+ 10 20 30 -PPPTIl 40 50 60 70 80 ■ | 90 ■ J । । 100 | ‘ 110 । | WWW VMMMwawwa #28161: Allyl mercaptan 41 74 3.20 ' 3.40 3.60 3.80 4.00— m/z 84.00 28.88% 5000-

47

m/z-> 0 -48314। 111,,53.59..99,, 10 50 60 70 20 30 40 1II/n/n/aIaa0a101)) 80 90 100 110 3.20 3.40 3.60 3.80 4.00

11383.D 050102.M Tue May 21 11:55:15 2002 Page 4

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