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GCMS instrument log for sample AE09654, May 2002

Machine-extracted title · confidence 95%

Instrument log and analysis summary for GCMS testing of sample AE09654 conducted on May 23, 2002.

NYC-WTC_000023745–000023753

Folder label: “GCMS X 5/9/02 A 5/20/02

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NYC 9/11 Public Portal Document LSC Area Percent Report . Data File : C:\HPCHEM\l\DATA\MAY2002\9654.D Vial: 12 Acq On : 20 May 2002 5:59 pm Operator: Sample : EXTRACTED 5/9 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 8.113 331 335 366 rVB 788929 1885470 72.44% 12.895% 2 12.145 769 775 790 rBV 813231 2036022 78.23% 13.925% 3 15.773 1165 1171 1189 rBV 1248692 2602654 100.00% 17.801% 4 21.079 1744 1750 1768 rBV 1227032 2519821 96.82% 17.234% 5 23.223 1976 1984 1993 rBV 564806 1115156 42.85% 7.627% 6 25.524 2228 2235 2246 rBV2 1025986 2165621 83.21% 14.812% 7 33.578 3107 3114 3129 rBV2 604292 1338964 51.45% 9.158% 8 37.784 3566 3573 3592 rBV2 341126 957502 36.79% 6.549%

Sum of corrected areas: 14621210 9654.D GCMS0520.M Tue May 21 11:38:16 2002

NYC-WTC_000023750

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NYC-WTC_000023750Source: NYC Law Department, mirrored locally

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