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GCMS instrument log for sample AE10065, May 2002

Machine-extracted title · confidence 95%

Instrument log and analysis summary for GCMS testing of sample AE10065 conducted on May 23, 2002.

NYC-WTC_000023728–000023737

Folder label: “GCMS X 5/9/02 A 5/20/02

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Scanned page image, NYC-WTC_000023733
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

. Data File : C:\HPCHEM\1\DATA\MAY2002\10065.D Vial: 16 Acq On : 20 May 2002 9:55 pm Operator: Sample : EXTRACTED 5/9 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.113 331 335 366 rVB 819746 1867343 64.63% 11.354% 2 9.919 528 532 545 rVB 15010 40608 1.41% 0.247% 3 12.145 769 775 793 rVB 935641 2239112 77.50% 13.615% 4 15.774 1165 1171 1189 rBV 1445049 2889206 100.00% 17.568% 5 21.080 1744 1750 1770 rBV 1410733 2831923 98.02% 17.219%

6 23.224 1975 1984 1994 rBV 724437 1453061 50.29% 8.835% 7 25.515 2228 2234 2244 rBV2 1157440 2490858 86.21% 15.145% 8 33.579 3107 3114 3130 rBV2 671300 1534717 53.12% 9.332% 9 37.785 3564 3573 3589 rBV2 381287 1099450 38.05% 6.685%

Sum of corrected areas: 16446278

10065.D GCMS0520.M Tue May 21 11:38:05 2002

NYC-WTC_000023733

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NYC-WTC_000023733Source: NYC Law Department, mirrored locally

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