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GCMS instrument log for sample AE10064, May 2002

Machine-extracted title · confidence 95%

Instrument log and analysis summary for GCMS testing of sample AE10064 conducted on May 23, 2002.

NYC-WTC_000023708–000023717

Folder label: “GCMS X 5/9/02 A 5/20/02

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Scanned page image, NYC-WTC_000023713
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

• Data File : C:\HPCHEM\1\DATA\MAY2002\10064.D Vial: 15 Acq On : 20 May 2002 8:56 pm Operator: Sample : EXTRACTED 5/9 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.112 331 335 367 rVB 771470 1830043 60.49% 10.722% 2 9.918 528 532 545 rVB 16432 45754 1.51% 0.268% 3 12.144 769 775 792 rVB 989172 2348435 77.62% 13.759% 4 15.773 1166 1171 1188 rBV 1487008 3025476 100.00% 17.726% 5 21.079 1744 1750 1763 rBV 1425307 2950512 97.52% 17.286%

6 23.223 1975 1984 1999 rBV 716678 1429555 47.25% 8.375% 7 25.523 2228 2235 2247 rBV2 1194817 2543408 84.07% 14.901% 8 33.578 3107 3114 3128 rBV 759283 1658423 54.82% 9.716% 9 37.784 3565 3573 3595 rBV2 423888 1236869 40.88% 7.247%

Sum of corrected areas: 17068475

10064.D GCMS0520.M Tue May 21 11:37:53 2002

NYC-WTC_000023713

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NYC-WTC_000023713Source: NYC Law Department, mirrored locally

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