GCMS instrument log for sample AE10065, May 2002

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Data File : C: \HPCHEM\ 1 \DATA\MAY2 002\10065.D Vial: 16 Acq On : 20 May 2002 9:55 pm Operator: Sample : EXTRACTED 5/9 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.11 33.36 ug/1 1867340 1,4-Dichlorobenzene-d4 12.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-me thy 1- 116 C6H1202 000123-42-2 64 2 CH2=CH:CH2C(O)OCH3 100 C5H802 003724-55-8 9 3 2,3-Bytanedione, monooxime 101 C4H7NO2 000057-71-6 7 4 Aceton.e 58 C3H6O 000067-64-1 7 Abundance Scan 335 (8.113 min): 10065.D (-) m/z 43.05 100.00% 43

5000 59

101 ■ ‘ i ' ■ ■ • i ■ ' m-' 1' 11 7.80 8.00 8.20 8.40 .......... 38,1 +53+ 0- > ■ i ■ । । ■ I । ■ i ■ ■ ‘ ; j । 69 83 | m/ z 59.10 39.21% rn/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 43

5000 59 7.80 8.00 8.20 8.40 m/z 58.10 16.02% 27 101 J H +49 + 6011* 83 m/z-> .......................... I I,, 10 20 30 40 50 70 80 90 00 100 110 Abundance #1448: CH2=CHCH2C(O)OCH3 43 7.80 8.00 8.20 8.40 5000 m/z 101.15 11.65%

38 + ——58 — 100 72 ————— miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1607:2,3-Butanedione, monooxime 43 /0 7.80 8.00 8.20 8.40 m/z 41.05 6.62% 5000

15 ....... I, ..... ,30 , 38 ' 1 i ' ' ' n 1 ' ■ ■ I' 1 ‘ 1 । 1 51 58 101

m/z—> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40

10065.D GCMS0520.M Tue May 21 11:38:07 2002 Page 1

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