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GC/MS analysis results, sample AE09770, May 15 2002

Machine-extracted title · confidence 100%

Laboratory report page showing GC/MS analysis for sample AE09770 including surrogate recovery data on May 15, 2002.

NYC-WTC_000023621–000023634

Folder label: “GCMS X 5/9/02 A 5/10/02

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Scanned page image, NYC-WTC_000023627
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\MAY1002\9770.D Vial: 12 Acq On : 10 May 2002 11:47 pm Operator: Sample : GC/MS SCAN 5/9 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.140 334 338 366 rBV 601746 1409892 30.44% 5.659% 2 12.163 771 777 796 rBV 1455634 3288376 71.00% 13.199% 3 15.801 1167 1174 1190 rBV 1974953 4121298 88.98% 16.542% 4 21.106 1746 1753 1776 rBV 2239902 4631716 100.00% 18.591% 5 23.251 1978 1987 1995 rBV 739929 1550426 33.47% 6.223% 6 25.221 2190 2202 2208 rBV3 35770 97622 2.11% 0.392% 7 25.551 2231 2238 2249 rBV2 1941390 4186594 90.39% 16.805% 8 26.513 2337 2343 2350 rBV 44165 90351 1.95% 0.363% 9 27.750 2473 2478 2486 rVB 42169 81036 1.75% 0.325% 10 28.932 2600 2607 2612 rBV 28688 60270 1.30% 0.242% 11 33.615 3111 3118 3133 rBV2 1274716 2982793 64.40% 11.973% 12 33.844 3138 3143 3151 rVB 19525 52268 1.13% 0.210% 13 37.848 3571 3580 3605 rBV2 784585 2360773 50.97% 9.476%

Sum of corrected areas: 24913415 9770.D GCMS0510.M Mon May 13 12:10:21 2002

NYC-WTC_000023627

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NYC-WTC_000023627Source: NYC Law Department, mirrored locally

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