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GCMS analysis results for sample AE10517, May 2002

Machine-extracted title · confidence 100%

GCMS analytical report for sample AE10517 showing unknown compounds and surrogate recovery data from May 21, 2002.

NYC-WTC_000045331–000045343

Folder label: “GCMS X 5/2/02 A 5/12/02

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Scanned page image, NYC-WTC_000045336
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\MAY1002\10517.D Vial: 40 ' Acq On : 12 May 2002 4:06 am Operator: Sample : gc/ms scan 5/2 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.138 334 338 367 rVB 506376 1172260 22.50% 4.269% 2 12.161 771 777 793 rBV 1656391 3729541 71.57% 13.582% 3 15.789 1167 1173 1190 rBV 2211926 4703310 90.26% 17.129% 4 21.095 1746 1752 1768 rBV 2398232 5210946 100.00% 18.977% 5 23.239 1978 1986 1993 rVB 230314 481164 9.23% 1.752%

6 23.853 2047 2053 2058 rBV 65153 118416 2.27% 0.431% 7 25.210 2194 2201 2209 rVB2 32212 92020 1.77% 0.335% 8 25.549 2230 2238 2249 rBV2 2134013 4836328 92.81% 17.613% 9 28.802 2588 2593 2596 rBV3 25865 61902 1.19% 0.225% 10 31.138 2842 2848 2865 rBV 883741 1771446 33.99% 6.451%

11 33.613 3110 3118 3133 rBV2 1353815 3154041 60.53% 11.486% 12 37.837 3570 3579 3597 rBV2 715451 2127353 40.82% 7.747%

Sum of corrected areas: 27458727

10517.D GCMS0510.M Thu May 16 15:10:26 2002

NYC-WTC_000045336

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NYC-WTC_000045336Source: NYC Law Department, mirrored locally

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