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GCMS reference analysis results for volatile organics, May 2002

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Laboratory report showing GC/MS reference analysis results for volatile organic compounds in sample AE10137 analyzed on May 14, 2002.

NYC-WTC_000023431–000023438

Folder label: “GCMS X 5/9/02 A 5/13/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) ? Data File : C:\MSDCHEM\1\DATA\051302\506REF1.D Vial: 7 Acq On : 13 May 2002 4:22 pm Operator: Mclean Sample : 5/9 kb Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: May 14 11:45:18 2002 Quant Results File: 050102.RES

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Mon May 13 11:40:29 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Compound R.T. Qlon Response Cone Unit Qvalue

36) Fluoroanthene 26.54 202 8207298 16.78 ug/L 98 3 8) Pyrene 27.17 202 8603931 18.78 ug/L 97 39) Butylbenzylphthalate 29.53 149 2353061 11.53 ug/L 94 40) Benzo(a)anthracene 30.79 228 5543566 15.20 ug/L 96 41) Bis(2-ethylhexyl)phthalate 31.39 149 2590258 9.39 ug/L 99 42) Chrysene 30.88 228 6486066m 17.18 ug/L 44) Di-n-octylphthalate 33.23 149 2050586m 6.65 ug/L 45) Benzo(b)fluoranthene 33.75 252 3795686 15.00 ug/L 97 46) Benzo(k)fluoranthene 33.82 252 6135829 19.29 ug/L 99 47) Benzo(a)pyrene 34.55 252 2868570m 11.35 ug/L 48) Indeno(1,2,3-cd)pyrene 37.39 276 1260424 7.12 ug/L 98 49) Dibenz(a,h)anthracene 37.51 278 2222949m 11.80 ug/L 50) Benzo(g,h,i)perylene 38.13 276 3140308m 15.88 ug/L

(#) = qualifier out of range (m) = manual integration (+) = signals summed 506REF1.D 050102.M Tue May 14 11:46:17 2002 Page 2

NYC-WTC_000023437

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NYC-WTC_000023437Source: NYC Law Department, mirrored locally

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