GCMS scan report for Method 508, April 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\l\DATA\020419\08430.D Vial: 17 Acq On : 19 Apr 2002 11:53 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 11 Undecanoic acid, 11-amino- Concentration Rank 16 R.T. EstConc Area Relative to ISTD R.T. 41.87 0.22 ug/1 372563 Perylene-dl2 43.16 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Undecanoic acid, 11-amino- 201 C11H23NO2 002432-99-7 1 2 Ethenamine, N-methyl-N-nitroso- 86 C3H6N20 004549-40-0 1 3 Aminocaproic Acid 131 C6H13N02 000060-32-2 1 4 1-Nonanamine 143 C9H21N 000112-20-9 1 Abundance Scan 6602 (41.869 min): 08430.D (-6558) (-) m/z 40.10 100.00%l 43

5000

73 86 96 149 163 41.60 41.80 42.00 42.20 I 49 i। 0 .................. ii 11 "'11111111' 1111 THHp 41.10 7.72% n/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #981: Undecanoic acid, 11 -amino- 33

5000 142 41.60 41.80 42.00 42.20 45 55 m/z 73.10 6.23% 73 86 100 114 129 0 —18.4 -mm , ■ ■ >'l156 171 185 200 ' ■ >' l ■ • ■ > I >' ■' I ■ l ■ • l ■ ■ ■11''" I iz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #737: Ethenamine, N-methyl-N-nitroso- 33 42

41.60 41.80 42.00 42.20 5000 m/z 149.00 5.57% 57 , 67 86 0.... + Hr mlz-> i0 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #790: Aminocaproic Acid 33 ' I 1 r' ' I 1 ’ ' I TI 41,60 41.80 42.00 42.20 m/z 96.00 5.15%| 5000

45 72 । 55 0 . । ।, 11. > "y,, /r 111 ri >'| > । m |i ... ।.8411, ।, 1111.., 114 131 , 11 ht[ 111111111111111111111111 p 1111 ।।।.,,, ■ ■ । ■ ' ■ । । > n/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 41,60 41.80 42.00 42.20

08430.D SCAN020418.M Mon Apr 29 08:29:51 2002 Page 26

NYC-WTC_000023251