GCMS scan report for Method 508, April 2002

NYC 9/11 Public Portal Document ’’LY**** **E

Data File : C:\MSDCHEM\l\DATA\020419\08430.D Vial: 17 Acq On : 19 Apr 2002 11:53 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 10 l-Methyl-9-chloro-acridine Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

40.44 0.26 ug/1 513037 Chrysene-dl2 39.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-Methyl-9-chloro-acridine 227 C14H10C1N 1000147-94-6 40 2 Phenol, 2-(2-benzothiazolyl)- 227 C13H9NOS 003411-95-8 33 3 5-Cyano-8-dimethylamino-6-methox... 227 C13H13N3O 1000213-20-5 33 4 1,3,5-Triazine-2,4-diamine, N-et... 227 C9H17N5S 000834-12-8 9 Abundance Scan 6359 (40.442 min): 08430. D (-6351) (-) m/z 227.20 100.00% 2227

5000 - 113 40.20 40.40 40.60 40.80

n/z-> 0- 40 51 69 86 99 ----- 20 40 60 80 100 .1.,.137 . 170.,..197.1 240 - 120 140 160 180 200 220 240 m/z 113.60 29.51% Abundance #89141:1-Methyl-9-chloro-acridine Z!7

X yha, I I I I I I I I 5000 192 M A

40.20 40.40 40.60 40.80 m/z 228.10 19.36% 75 96 0- 10)00* "re • "" 1‘* 1 ‘"I 1 i"1"1 i t, 1- -- 114 126 139 152 164 179 . miz-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #127060: Phenol, 2-(2-benzothiazolyl)- Z!7 ----- 40.20 40.40 40.60 40.80 5000 199 m/z 226.10 14.23% 69 39 86 99

miz-> 0- 15,27,1157 20 40 ,4.4113,127 1401547106 — I. 60 80 100 120 140 160 180 200 220 240 Abundance #89117:5-Cyano-8-dimethylamino-6-methoxyquinoIine 22.7 40.20 40.40 40.60 40.80 212 m/z 225.10 12.75%

5000

198

/z-> 0 42 63 76 88 101 114 127 141 155 169 184 | • • | ■ ■ < ■ | । l 1 ■ ("* । I T'| 1 1 I I | l ■ >| > < I I | I I I I | I I* I I J T I 1 1 1 1"

20 40 60 80 100 120 140 160 180 200 '1 1 1 । । । 1 1 1 M..... 220 240 40.20 40.40 40.60 40.80

08430.D SCAN020418.M Mon Apr 29 08:29:50 2002 Page 25

NYC-WTC_000023250