GCMS analysis results for sample AE09573, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\MSDCHEM\1\DATA\050902\9572.D Vial: 9 Acq On 9 May 2002 9:48 pm Operator: Mclean Sample 5/8 kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHCDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 3 Acetone Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

7.73 0.35 ug/L 412513 1,4-Dichlorobenzene-d4 9.94

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Acetone 58 C3H60 000067-64-1 9 2 3-Pyrrolidinol 87 C4H9NO 040499-83-0 3 5-Hexen-2-one 98 C6H10O 000109-49-9 9 4 Propane, 1-(1-methylethoxy)- 102 C6H140 000627-0847 9 Abundance Scan 791 (7.727 min): 9572. D (-784) (-) 43

5000 58

.......... Il 87 98 1 ' i ' ■ • i ‘ ‘ ■ i 7.40 7.60 7.80 8.00 .I...... I,,,, m/z-> 01 .................. 0 10 20 30 3ll40 50 60 70 80 90 100 m/ Z 58.10 31.04% Abundance #109123: Acetone 43 MVAW MwAW/w 5000 ' ' I 1 ‘ 1 ‘ I ' ‘ ' I 15 7.40 7.60 7.80 8.00 58 m/ Z 87.10 17.57% 27 2 0- 1 ' ' i 1 1 m/z-> 6' 10 20 30 40 50 60 70 80 90 100 Abundance #4163:3-Pyrrolidinol 43 ............. ............. A 7.40 7.60 7.80 8.00 5000 m/z 59.10 14.58% 87 57 68

m/z-> 01 1 ■ i ■ ■ ' ■ i ■ ■ ■ ■ i ' 1 1 ■ i ■ 1 ■ ' i 1 0 10 20 30 40 —5051all77 60 70 80 ------ 90 100 Abundance #5001:5-Hexen-2-one 43 .......... Ill......l)., 7.40 7.60 7.80 8.00 m/z 83.10 11.19%

5000

55 15 27 0 I [l|l , 371,1, 490 1 1 । 1 1 11 । 1,1 111 111i1111 r1 Hr । 65 71 77 83 । । । । ■ । । । । ■ । । । । । ।' । 98 I 1....... 1.1 ' ' I ' ' ‘ ‘ I m/z-> 0 10 20 30 40 50 60 70 80 90 100 7.40 7.60 7.80 8.00

9572.D 050102.M Mon May 13 11:49:06 2002 Page 6

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