GCMS analysis results for sample AE09571, May 2002

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88 27.263 4107 4116 4124 W 9 41380 2125100 2.92% 0.331% 89 27.322 4124 4126 4129 W 4 32845 586678 0.81% 0.091% 90 27.392 4133 4138 4140 W 6 33737 706091 0.97% 0.110%

91 27.410 4140 4141 4152 W 6 33180 1401637 1.93% 0.218% 92 27.492 4152 4155 4160 W 7 33065 834248 1.15% 0.130% 93 27.545 4160 4164 4178 W 7 37823 2243585 3.08% 0.349% 94 27.692 4178 4189 4197 W 7 42950 2614465 3.59% 0.407% 95 27.751 4197 4199 4201 W 3 36975 488542 0.67% 0.076%

96 27.768 4201 4202 4215 W 3 37134 1625855 2.23% 0.253% 97 27.862 4215 4218 4221 W 5 32050 626601 0.86% 0.098% 98 27.903 4221 4225 4228 W 5 32465 797821 1.10% 0.124% 99 27.968 4228 4236 4245 W 5 41833 2142748 2.94% 0.334% 100 28.050 4245 4250 4254 W 8 39198 1221578 1.68% 0.190%

101 28.121 4254 4262 4275 W 8 39122 2678243 3.68% 0.417% 102 28.215 4275 4278 4280 W 4 35351 628994 0.86% 0.098% 103 28.238 4280 4282 4285 W 4 34053 595478 0.82% 0.093% 104 28.309 4285 4294 4303 W. 4 47938 2566595 3.53% 0.400% 105 28.373 4303 4305 4306 W 2 39711 476565 0.65% 0.074%

106 28.391 4306 4308 4319 W 8 40935 1648441 2.26% 0.257% 107 28.491 4322 4325 4331 W 6 36266 1046037 1.44% 0.163% 108 28.573 4331 4339 4349 W 6 40824 2340992 3.22% 0.365% 109 28.685 4349 4358 4362 W 6 37047 1622630 2.23% 0.253% 110 28.738 4362 4367 4370 W 7 34727 972494 1.34% 0.151%

ill 28.767 4370 4372 4380 W 8 35940 1212012 1.66% 0.189% 112 28.902 4390 4395 4399 W 8 34111 1037050 1.42% 0.162% 113 28.973 4403 4407 4408 W 4 32558 636397 0.87% 0.099% 114 29.061 4417 4422 4426 W 7 36131 998967 1.37% 0.156% 115 29.090 4426 4427 4430 W 3 35026 535410 0.74% 0.083%

116 29.184 4430 4443 4448 W 3 41592 2400498 3.30% 0.374% 117 29.231 4448 4451 4465 W 3 37969 2102241 2.89% 0.327% 118 29.355 4465 4472 4474 W 8 34004 974728 1.34% 0.152% 119 29.431 4474 4485 4494 W 8 36755 2503816 3.44% 0.390% 120 29.519 4494 4500 4508 W 8 37199 1622301 2.23% 0.253%

121 29.654 4520 4523 4533 W 8 31090 1323478 1.82% 0.206% 122 29.760 4533 4541 4546 W 10 30738 1417881 1.95% 0.221% 123 29.831 4551 4553 4555 W 3 30635 397368 0.55% 0.062% 124 29.889 4559 4563. 4565 W 5 30166 576325 0.79% 0.090% 125 29.913 4565 4567 4570 W 4 30065 561522 0.77% 0.087%

126 29.983 4570 4579 4586 W 4 37389 1713793 2.35% 0.267% 127 30.042 4586 4589 4590 W 3 31596 520925 0.72% 0.081% 128 30.089 4590 4597 4610 W 3 33294 2238138 3.07% 0.349% 129 30.195 4610 4615 4617 W 6 31797 744778 1.02% 0.116% 130 30.230 4617 4621 4627 W 9 31926 1028703 1.41% 0.160%

131 30.277 4627 4629 4641 W 9 32315 1572985 2.16% 0.245% 132 30.383 4641 4647 4648 W 6 30142 740140 1.02% 0.115% 133 30.400 4648 4650 4652 W 3 30907 369182 0.51% 0.058% 134 30.494 4652 4666 4674 W 3 33206 2432534 3.34% 0.379% 135 30.547 4674 4675 4677 W 2 31965 344244 0.47% 0.054%

136 30.577 4677 4680 4682 W 4 33735 614270 0.84% 0.096% 137 30.600 4682 4684 4688 W 5 32376 630715 0.87% 0.098%

9570.D 050102.M Mon May 13 11:46:44 2002 Page 3

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