GCMS analysis results for sample AE09571, May 2002

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138 30.647 4688 4692 4696 W 6 34079 965638 1.33% 0.150% 139 30.812 4696 4720 4748 W 2 2565581 69541848 95.52% 10.832% 140 31.035 4748 4758 4768 W 2 50822 3340727 4.59% 0.520%

141 31.106 4768 4770 4775 W 6 48219 1261428 1.73% 0.196% 142 31.158 4775 4779 4787 W 10 45680 1792179 2.46% 0.279% 143 31.217 4787 4789 4792 W 4 43654 786934 1.08% 0.123% 144 31.247 4792 4794 4797 W 4 43130 689993 0.95% 0.107% 145 31.276 4797 4799 4803 W 5 43160 879164 1.21% 0.137%

146 31.335 4803 4809 4811 W 7 45404 1262335 1.73% 0.197% 147 31.388 4811 4818 4831 W 7 59132 3808004 5.23% 0.593% 148 31.470 4831 4832 4837 W 5 54655 1153323 1.58% 0.180% 149 31.511 4837 4839 4841 W 3 51409 736905 1.01% 0.115% 150 31.546 4841 4845 4846 W 3 53232 941537 1.29% 0.147%

151 31.570 4846 4849 4853 W 6 54086 1283646 1.76% 0.200% 152 31.605 4853 4855 4861 W 7 56012 1524078 2.09% 0.237% 153 31.664 4861 4865 4871 W 8 54072 1865234 2.56% 0.291% 154 31.711 4871 4873 4875 W 3 52870 781942 1.07% 0.122% 155 31.752 4875 4880 4882 W 6 53500 1180601 1.62% 0.184%

156 31.787 4882 4886 4892 W 9 54632 1907929 2.62% 0.297% 157 31.863 4896 4899 4904 W 7 54017 1521092 2.09% 0.237% 158 31.916 4904 4908 4912 W 7 53844 1520921 2.09% 0.237% 159 31.963 4912 4916 4921 W 8 54659 1676552 2.30% 0.261% 160 32.046 4921 4930 4941 W 8 62693 4098133 5.63% 0.638%

161 32.116 4941 4942 4949 W 7 59310 1696594 2.33% 0.264% 162 32.175 4949 4952 4954 W 4 59591 1002928 1.38% 0.156% 163 32.193 4954 4955 4958 W 3 58025 781662 1.07% 0.122% 164 32.245 4958 4964 4966 W 7 58787 1592917 2.19% 0.248% 165 32.316 4966 4976 4978 W 7 62210 2566186 3.52% 0.400%

166 32.375 4978 4986 4998 W 7 70736 4785135 6.57% 0.745% 167 32.457 4998 5000 5002 W 3 64624 740796 1.02% 0.115% 168 32.480 5002 5004 5007 W 4 66577 1281028 1.76% 0.200% 169 32.539 5007 5014 5017 W 9 70592 2375102 3.26% 0.370% 170 32.569 5017 5019 5023 W 5 72845 1603672 2.20% 0.250%

171 32.621 5023 5028 5030 W 6 72842 1602332 2.20% 0.250% 172 32.639 5030 5031 5041 W 9 72433 2729435 3.75% 0.425% 173 32.704 5041 5042 5059 W 9 71221 4363021 5.99% 0.680% 174 32.821 5059 5062 5072 W 10 67406 3060905 4.20% 0.477% 175 32.886 5072 5073 5076 W 3 66832 973087 1.34% 0.152%

176 32.939 5076 5082 5089 W 3 68494 3127525 4.30% 0.487% 177 33.009 5089 5094 5097 W 7 70282 1759542 2.42% 0.274% 178 33.033 5097 5098 5103 W 5 67004 1484389 2.04% 0.231% 179 33.074 5103 5105 5108 W 4 68110 1108514 1.52% 0.173% 180 33.103 5108 5110 5112 W 3 65239 911481 1.25% 0.142%

181 33.127 5112 5114 5118 W 5 66173 1478828 2.03% 0.230% 182 33.238 5128 5133 5134 W 5 64876 1330074 1.83% 0.207% 183 33.285 5134 5141 5144 W 8 77232 2668470 3.67% 0.416% 184 33.315 5144 5146 5158 W 8 72019 3395438 4.66% 0.529% 185 33.397 5158 5160 5164 W 5 66358 1337552 1.84% 0.208%

186 33.438 5164 5167 5168 W 3 63766 830066 1.14% 0.129% 187 33.473 5168 5173 5175 W 6 66864 1577569 2.17% 0.246%

9570.D 050102.M Mon May 13 11:46:44 2002 Page 4

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