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GCMS blank analysis results for May 2002

Machine-extracted title · confidence 100%

Laboratory report of a GCMS blank run conducted on May 14, 2002, showing non-detect results for various compounds.

NYC-WTC_000022965–000022989

Folder label: “GCMS X 5/8/02 A 5/9/02

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Scanned page image, NYC-WTC_000022983
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NYC 9/11 Public Portal Document LLOLdry bedrcn compound Keporc

Data File C:\MSDCHEM\1\DATA\050 9 02\05 0 8LB.D Vial: 4 Acq On 9 May 2002 5:43 pm Operator: Mclean Sample 5/8 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 12 Trisiloxane, 1,1,1,5,5,5-he... Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 34.37 0.89 ug/L 573160 Perylene-dl2 34.70 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H3604Si5 003555-47-3 38 2 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H3604Si5 003555-47-3 38 3 Mercaptoacetic acid, bis(trimeth... 236 C8H20O2SSi2 006398-62-5 37 4 1,2-Benzenedicarboxylic acid, bi... 310 C14H2204Si2 002078-22-0 35 Abundance Scan 5325 (34.367 min): 0508LB.D (-5316) (-) m/z 73.10 100.00% 73 147 221 ft 5000 281 355 - 429

m/z-> 0— 0 -LL 50 100 150 191 | 200 250 300 1,327, 1 , . 401 , 1 . 350 400 34 00 34,20 34.40 34.60 34.80 m/z 147.10 74.93% Abundance #115144: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trim... 73 147

5000 113 1 i ■ ' ' ■ i ■

281 34.00 34.20 34.40 34.60 34.80 45 m/Z 221.10 66.34%

O—T I, ' i 1 117 207 249 t I ll

/z-> 0 50 100 150 200 250 300 Abundance #26961: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trime... 73 147 ---------- 281 34.00 34.20 34,40 34.60 34.80 5000 m/z 281.10 35.56%

369 O-T 45 | . ■ i 1 95 117 1—— 1"9 .177.27..249, . 310 341 .. n/z-> 0 50 100 150 200 250 300 350 400 Abundance #26922: Mercaptoacetic acid, bis(trimethylsilyl)- AAAA,AAAA,AAMMALMA,AADMAAM 73 34.00 34.20 34.40 34.60 34.80 147 m/z 355.10 28.28%| 5000 221 45 0 1, 13 . 1 11 104 1 1 ' 1 1 ’ 1 ‘i + r' " , i 169193 , | , - m/z-> 0 50 100 150 200 250 300 350 400 34.00 34.20 34.40 34.60 34.80

0508LB.D 050102.M Tue May 14 10:15:00 2002 Page 15

NYC-WTC_000022983

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NYC-WTC_000022983Source: NYC Law Department, mirrored locally

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