NYC 9/11 Public Portal Document
LLOLdry bedrcn compound Keporc
Data File C:\MSDCHEM\1\DATA\050 9 02\05 0 8LB.D Vial: 4
Acq On 9 May 2002 5:43 pm Operator: Mclean
Sample 5/8 kb Inst Instrumen
Mise Multiplr: 1.00
MS Integration Params: LSCINT.e
Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator)
Title : 508 Modified GC/MS scan
Library : C:\DATABASE\NIST98.L
Peak Number 12 Trisiloxane, 1,1,1,5,5,5-he... Concentration Rank 7
R.T. EstConc Area Relative to ISTD R.T.
34.37 0.89 ug/L 573160 Perylene-dl2 34.70
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H3604Si5 003555-47-3 38
2 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H3604Si5 003555-47-3 38
3 Mercaptoacetic acid, bis(trimeth... 236 C8H20O2SSi2 006398-62-5 37
4 1,2-Benzenedicarboxylic acid, bi... 310 C14H2204Si2 002078-22-0 35
Abundance Scan 5325 (34.367 min): 0508LB.D (-5316) (-) m/z 73.10 100.00%
73
147
221
ft
5000
281
355 -
429
m/z->
0—
0
-LL
50 100 150
191 |
200 250 300
1,327, 1 , . 401 , 1 .
350 400
34 00 34,20 34.40 34.60 34.80
m/z 147.10 74.93%
Abundance #115144: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trim...
73
147
5000 113 1 i ■ ' ' ■ i ■
281 34.00 34.20 34.40 34.60 34.80
45 m/Z 221.10 66.34%
O—T I,
' i 1
117 207 249
t I ll
/z-> 0 50 100 150 200 250 300
Abundance #26961: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trime...
73 147
----------
281 34.00 34.20 34,40 34.60 34.80
5000 m/z 281.10 35.56%
369
O-T
45
| .
■ i 1
95 117
1—— 1"9
.177.27..249, . 310 341 ..
n/z-> 0 50 100 150 200 250 300 350 400
Abundance #26922: Mercaptoacetic acid, bis(trimethylsilyl)- AAAA,AAAA,AAMMALMA,AADMAAM
73 34.00 34.20 34.40 34.60 34.80
147
m/z 355.10 28.28%|
5000
221
45
0 1, 13 . 1 11 104
1 1 ' 1 1 ’ 1 ‘i + r' "
, i 169193 , | , -
m/z-> 0 50 100 150 200 250 300 350 400 34.00 34.20 34.40 34.60 34.80
0508LB.D 050102.M Tue May 14 10:15:00 2002 Page 15
NYC-WTC_000022983
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