NYC 9/11 Public Portal Document
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Data File : C:\MSDCHEM\1\DATA\051702\11380.D Vial: 7
Acq On : 17 May 2002 5:40 pm Operator: Mclean
Sample : 5/15 ad Inst Instrumen
Mise Multiplr: 1.00
MS Integration Params: LSCINT.e
Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator)
Title : 508 Modified GC/MS scan
Library : C:\DATABASE\NIST98.L
Peak Number 13 3,6-Dioxa-2,4,5,7-tetrasila... Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
39.32 0.98 ug/L 699861 Perylene-dl2 34.70
Hit# of 5 Tentative ID MW MolForm CAS# Qual
l 3,6-Dioxa-2,4,5,7-tetrasilaoctan . .. 294 C10H3002Si4 004342-25-0 43
2 3-Isopropoxy-1,1,1,7,7,7-hexamet... 576 C18H5207Si7 071579-69-6 38
3 Mercaptoacetic acid, bis(trimeth... 236 C8H20O2SSi2 006398-62-5 37
4 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H3604Si5 003555-47-3 35
Abundance Scan 6169 (39.326 min): 11380.D (-6156) (-) m/z 73.05 100.00%
73
147
221
5000
281 355 MWMARMA WW
429
193 39.00 39.20 39.40 39.60
m/z->
0-
0
4950 100 150 200 1 1 i
i
250
.1 ।' । i । ' 11 > ■ ■ ■ ।
300 350 400 450 500
■
■ । ' ■ 1 1 । 1 1 1 ■ i ' •
550
m/z 147.10 79.15%
Abundance #87890: 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7...
147 221
73
A A______ IA A
5000 ' ’ 1 1 1 '“T r"
39.00 39.20 39.40 39.60
191 m/Z 221.10 72.40%
JU
117 279
45 ,, 1 249 |
0-1T 1 ''11 1 ' i ' "■ ■ i r 1 1 1 i 1 1
m/z-> 0 50 100 150 200 250 300 350 400 450 500 550
Abundance #26784: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(tri...
73
■ 1 i 1 1 ■ 1 i
39.00 39.20 39.40 39.60
5000 m/Z 281.00 36.65%
147
43 221 281 327 415 519 561
1 1
Ti/z->
0-
0 50
■ ■ i ■ ■ ■■ ■ 1 i ■ ■
100 150 200 250 300 350 400 450 500 550 Wmlpy
Abundance #26922: Mercaptoacetic acid, bis(trimethylsilyl)-
73 39.00 39.20 39.40 39.60
147 m/z 207.00 35.13%
5000 uwWpAAw"wwoospuk
221
45
193
0-
13. 1L | r r 104
I ' '
1.
m/z-> 0 50 100 150 200 250 300 350 400 450 500 550 39.00 39.20 39.40 39.60 1
11380.D 050102.M Mon May 20 15:46:53 2002 Page 16
NYC-WTC_000025125
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