GCMS calibration table review, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APR2 502\9331.D Vial: 8 Acq On : 25 Apr 2002 7:32 pm Operator: Sample : gc/ms scan 4/18 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 3(2H)-Pyridazinone, 4,5-dihydr Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

8.24 0.79 ug/1 124776 1,4-Dichlorobenzene-d4 12.21

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3(2H)-Pyridazinone 4,5-dihydro-6-m 112 C5H8N20 005157-08-4 10 2 Acetamide, N-[(8. pha.,9R)-9-hydro 381 C22H27N3O3 056847-12-2 9 3 1-Fluorononane 146 C9H19F 000463-18-3 9 4 3-Pentyn-2-one, ,5-diethoxy- 170 C9H14O3 055402-04-5 4 Abundance Scan 348 (8.244 min): 9331 .D (-) m/z 42.95 100.00% 43 A 5000 125 97 85 — 63 119

m/z-> 20 ' i 1 JL50 60 70 80 1 1 I । 1 1 1 I I'l ' 1 I । । 90 100 110 | 120 130 8.00 m/z 124.95 8.20 8.40 8.60 42.34% Abundance #2490:3(2H)-Pyridazinone, 4,5-dihydro-6-methyl- 27 39 112 5000 8.00 8.20 8.40 8.60 56 50 m/ z 96.95 A 31.72% 84 ■ i ■ 1 ■ ■ i 1 ■ ■ ■ i ■ '

m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #52279: Acetamide, N-[(8.alpha.,9R)-9-hydroxy-6'-methoxycin 33 43 8.00 1 8.20 ........ 8.40 8.60 59 5000 50 m/z 46.95 22.74% 85

m/z-> - 20 30 40 150 70 —TuumTTT 60 70 80 90 —wTmOIE—TTT 100 110 120 130 Abundance #8922:1-Fluorononane 43 8.00 8.20 8.40 8.60 m/z 84.85 20.77% 5000 56 27 70 84 97

33 1 ■ । > I । •r • > । l ■ ■ i ■ • ■ ‘ i 1 ----- m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 8.00 8.20 8.40 8.60

9331.D GCMS0412.M Fri Apr 26 08:18:37 2002 Page 2

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