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← Document results/DEP Box 18/GCMS X 5/8/02 A 5/10/02
Document / 7 pages

GCMS calibration table review, May 2002

Machine-extracted title · confidence 100%

Reviewed data file listing retention times and response factors for deuterated internal standards.

NYC-WTC_000022750–000022756

Folder label: “GCMS X 5/8/02 A 5/10/02

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Scanned page image, NYC-WTC_000022753
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\MAYO3 0 2\LBB.D Vial: 27 Acq On 4 May 2002 5:32 pm Operator: Sample GC/MS SCAN 4/26 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.162 337 341 366 rBV 464485 1045809 30.35% 5.977% 2 12.194 775 781 797 rBV 1090576 2487767 72.21% 14.217% 3 15.822 1171 1177 1190 rBV 1502337 3135284 91.00% 17.918% 4 21.137 1750 1757 1773 rBV 1643401 3445388 100.00% 19.690% 5 23.272 1983 1990 1999 rVB 102293 202816 5.89% 1.159%

6 25.572 2234 2241 2252 rBV2 1480812 3191700 92.64% 18.240% 7 33.636 3113 3121 3140 rBV2 992339 2199101 63.83% 12.568% 8 33.856 3140 3145 3158 rVB 66898 162659 4.72% 0.930% 9 37.861 3574 3582 3596 rBV2 543297 1627764 47.24% 9.302%

Sum of corrected areas: 17498288

LBB.D GCMS0501.M Tue May 07 12:01:54 2002

NYC-WTC_000022753

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NYC-WTC_000022753Source: NYC Law Department, mirrored locally

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