NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\l\DATA\02MAR26\7113.D Vial: 7
Acq On 26 Mar 2002 8:47 pm Operator: 201-wb
Sample nyc Inst : GC/MS Ins
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\HP031802.M (RTE Integrator)
Title : VOCs BY EPA METHOD 524
Library : C:\DATABASE\NBS75K.L
Peak Number 2 Vanadium, (.eta.7-cycloheptatr Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
17.98 0.04 ug/L 15076 1,4-DIFLUOROBENZENE 15.12
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Vanadium, (.eta.7-cycloheptatrienyl 207 C12H12V 012636-68-9 2
2 5-Acetamido-4,7-dioxo-4,7-dihydrobe 207 C8H5N3O4 000000-00-0 2
3 Stannane, tetraethyl- 236 C8H20Sn 000597-64-8 1
4 Trimethylsilyl dipropylphosphinate 222 C9H23O2PSi 000000-00-0 1
w
Abundance Scan 823 (17.980 min): 7113.D (-) m/z 207.15 100.00%
207
9000
8000
70001 1 ■ i '
44
yo i ■ ■ ■ ' i 1
17.60 17.80 18.00 18.20
m/z 43.95 69.96%
TT
■ i ' ' ■ 1 i ■ ' ■ 1 i 1 ■ ' ■ i ' ■ ' ■ i 1 1 1 1 I 1 1 1 1 I 1 1 1 1 I 1 1 1 1 I 1 1 1 1 1 1
m/z-> 40 60 80 100 120 140 160 180 200 220 240
Abundance #24588: Vanadium, (.eta.7-cycloheptatrienylium)(.eta.5-2,4-
267
5000
51
116
129
v=w
17.60 17.80 18.00 18.20
3964 |. J
76 90 .142.. 181.....
' ' i ' ■ i ■ ■ ■ । i > ■ ■
m/Z->_____ 40______ __________________________________
60 80 100 120 140 160 180 200 220 240
Abundance #24499:5-Acetamido-4,7-dioxo-4,7-dihydrobenzofurazan
43
5000
207
68|, 165 179|
149 |
—PT ■ i ■ " 1 ■ i 851 1 1 ' i 107 130
■ ' 1 1 i 1 1 ■ ■ i ' ■ i ' 1 1 ' r 1 1 1 i 1
1 1 1 1 1 1 1 1 1
/z-> 40 60 80 100 120 140 160 180 200 220 240
Abundance #71065: Stannane, tetraethyl-
207
179
121
5000- 151
100
— , , , , 11, 134 ,, - 236
. TIT
■ । ■ ■ ■ ■ i ■ > > ■ । ■
m/z-> 40 60 80 100 120 140 160 180 200 220 240
7113.D HP031802.M Wed Mar 27 09:37:45 2002 Page 2
NYC-WTC_000022466
OCR can misread numbers and units. Confirm readings against the page image before using them.