Volatile organic compounds analysis results, March 26, 2002

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Data File : C:\HPCHEM\1\DATA\O2MAR26\7109.D Vial: 5 Acq On : 26 Mar 2002 5:11 pm Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP031802.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Vanadium, (.eta.7-cycloheptatr Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

17.93 0.04 ug/L 16671 1,4-DIFLUOROBENZENE 15.09

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Vanadium,(.eta.7-cycloheptatrienyl 207 C12H12V 012636-68-9 2 2 5-Acetamido-4,7-dioxo-4,7-dihydrobe 207 C8H5N3O4 000000-00-0 2 3 Stannane, tetraethyl- 236 C8H20Sn 000597-64-8 1 4 Trimethylsilyl dipropylphosphinate 222 C9H23O2PSi 000000-00-0 1 Abundance Scan 819 (17.929 min): 7109.D (-) m/z 207.15 100.00% 207

8000

■ ■ i ' 1 ' ■ i 1 1 1 i ■ 1 1 ' । 6000- 17.60 17.80 18.00 18.20 ,44... ............ m/z 44.05 53.24% m/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #24588: Vanadium, (.eta.7-cycloheptatrienylium)(.eta.5-2,4- 207

129 —— 51 5000- 116 17.60 17.80 18.00 18.20

39 , 64 76L 90,| 1,42 181 1 1 'i ■ ■ < • i 1 • ' i । ■ ■ • ■ । • । i ■ > ■ ■ | । । ■ ■ ■ ■ । ‘ i ■ ■ ■ ■ I ■ ■ ■ ■ i r m/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #24499: 5-Acetamido-4,7-dioxo-4,7-dihydrobenzofurazan 43

5000

207 68 165 179 1. 85 107 130 149 | | * TTr -T-p-Vr-r-p-r-r-r-r-p- m/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #71065: Stannane, tetraethyl- 207 - 179

121 5000- 151

100

m/z-> > 1 p ■ 1 > । 1 1 1 1 i ■ 40 60 80 mr 134 , ............ ......... 236 100 120 140 160 180 200 220 240

7109.D HP031802.M Wed Mar 27 09:41:08 2002 Page 1

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