Volatile organic compounds blank analysis results, March 22, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\02mar22\6590.D Vial: 6 Acq On : 22 Mar 2002 7:12 pm Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP031802.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L Peak Number 1 Hydrazine, 1,2-diethyl- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 15.75 0.03 ug/L 12532 1,4-DIFLUOROBENZENE 15.08 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Hydrazine, 1,2-diethyl- 88 C4H12N2 001615-80-1 4 2 1,3-Dioxolan-2-one 88 C3H403 000096-49-1 4 3 Sulfide, allyl methyl 88 C4H8S 010152-76-8 4 4 1,2 -Hydrazinedicarboxaldehyde 88 C2H4N202!000628-36-4 4 Abundance Scan 692 (15.748 mln): 6590.D (-) m/z 114.15 100.00% 1 4

5000 63 88 < i > • • < i > > ■ 1 I 1 1 1 ■ i ‘ 15.40 15.60 15.80 16.00 44 m/z 62.95 27.35% ' ■ i ■ ■ ■ ■ i ■' ■ ■ i ■ ■ ■ ■ i •' ■' i1''' i ■ ■ ■ ■ i'''' i'' 11''111 " ' I' ■ • i >» n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #840: Hydrazine, 1,2-diethyl- 31 59 88

5000 1 I 1 1 1 ' I ' 1 i ■ 1 ■ ■ i • ■ ■ ■ i ■ 44 73 15.40 15.60 15.80 16.00 m/z 88.00 26.96% n m/z-> 10 20 I 30 1 40 50 60 70 80 90 i

100 110 120 Abundance #62893:1,3-Dioxolan-2-one 29

43 88 15.40 15.60 15.80 16.00 5000 15

58... 73 I.. i. 11 ■ ।.. — 1 .. i...I 11 ■'' • i' ■'. i' ■ 11.... । ■ 1111 ■ Tor 111 w*rhH" m/z 44.05 10.93%

m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #62927: Sulfide, allyl methyl 41 15.40 15.60 15.80 16.00

73 88 5000

61 *— ‘ ' I ' ‘ ‘' I ‘ ‘ ' 1 . . 1 'I' m/z--> 10 20 30 40 50 60 70 80 90 100 110 120

6590.D HP031802.M Fri Mar 22 19:52:37 2002 Page 1

NYC-WTC_000022248