Volatile organic compounds results, Mar 6 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\l\DATA\02MAR06\04802.D Vial: 15 Acq On 7 Mar 2002 2:02 am Operator: 201-wb Sample nyc Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP022702.M (RTE Integrator) Title : VOCS BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Hydrazine, 1,2-diethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 15.73 0.03 ug/L 22662 1,4-DIFLUOROBENZENE 15.09 Hit# of 5 Tentative ID MW MolForm CAS# Qual. 1 Hydrazine, 1,2-diethyl- 88 C4H12N2 001615-80-1 4 2 1,3-Dioxolan-2-one 88 C3H403 000096-49-1 4 3 1,2-Hydraz inedicarboxaldehyde 88 C2H4N202! 000628-36-4 4 4 Sulfide, allyl methyl 88 C4H8S ______ 010152-76-8 3 Abundance Scan 690 (15.732 min): 04802.D (-) m/z 114.05 100.00% 1 4

5000

63 88 1 ‘ i ■ ■ ' ■ i ■ • ' i ' ■ ■1 i 15.40 15.60 15.80 16.00 44 12217 m/z 63.05 26.66% 4*1***‘I**3*I****/1** i ■ • ■ ’ i ’ ‘ • ■ i' m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #840: Hydrazine, 1,2-diethyl- 31

59 88 . ... ....... .... 5000 44 73 15.40 15.60 15.80 16.00 m/z 88.00 25.53%

• • l • • • • I • • । MU I “ " " I “ mmmpn m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #62893:1,3-Dioxolan-2-one 29 43 88 15.40 15.60 15.80 16.00 5000 m/z 43.95 10.77%

15 WM/wA 58 I' । p ।'11111 —d i ■ ■ i ■ ■ •111 ■ ■ ■ • i 73 ■' ■ ■ i ■1 i ■ ■ ■ ■ i ■ ■ ■' i ■ ■ ■11'1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #781:1,2-Hydrazinedicarboxaldehyde 31 15.40 15.60 15.80 16.00 ''' 60 88 5000

44 17

n/z-> r-p-m-p 10 20 1. 40Ill.. 30 . T-r-p-n-r-p-r 50 60 70 80 90 100 110 120 i' ■' ‘ i ■' ■ ■ i ‘ ' i ■'

04802.D HP022702.M Thu Mar 07 08:44:33 2002 Page 1

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