Volatile organic compounds results, Mar 4 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\02MAR04\04032.D Vial: 6 Acq On : 4 Mar 2002 1:45 pm Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP022702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L Peak Number 2 Hydrazine, 1,2-diethyl- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 15.77 0.04 ug/L 23735 1,4-DIFLUOROBENZENE 15.10 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Hydrazine, 1,2-diethyl- 88 C4H12N2 001615-80-1 4 2 l,3-Dioxolan-2-one 88 C3H403 000096-49-1 4 3 1,2-Hydrazinedicarboxaldehyde 88 C2H4N2021 000628-36-4 4 4 Sulfide, allyl methyl 88 C4H8S ________ 010152-76-8 3 Abundance Scan 693 (15.765 min): 04032.D (-) m/z 114.15 100.00%l 1 4

5000

63 15.40 15.60 15.80 16.00 1' i' ‘ ‘ ‘ i ‘ ‘ ‘ ‘ I ‘ 44 I ‘ i' ‘ ‘ ■ i ■ ■ ‘ ‘ i' ‘ • * 1 1 ‘ 11 1 1 1 ■ i ■ ■ • • i1 '11'1 m/z 88.10 24.60% m/z-> 10 20 30 40 50 60 70 80 100 110 120 Abundance #840: Hydrazine, 1,2-diethyl- 31 59 88

5000 ‘1 ‘24/1/6/1/01/3 44 73 15.40 15.60 15.80 16.00 m/z 63.05 23.50 — _______________ •n-j-TT-rr-p-r 121—001/0/ 1I’ 1111—001/721733 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #62893:1,3-Dioxolan-2-one 29

■ I' ■' ■ i ■ ■ 1 1 1 1 ■ ' 1 i ' 43 88 15.40 15.60 15.80 16.00 5000 m/z 44.05 11.69? 15 AMww 58 PP j_____ 73 1’11-11111153 ‘‘ 11 ।1 ‘ ।1 • i " 1 ■ i ■11 ■ i ■ ■111'1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #781:1,2-Hydrazinedicarboxaldehyde 31 15.40 15.60 15.80 16.00

60 88 5000

44 17

1 • 11 11 TT-p-r-n-p-r m/z--> 10 20 30 40 50 60 70 80 90 100 110 120

04032.D HP022702.M Tue Mar 05 08:22:08 2002 Page 2

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