Volatile organic compounds results, Mar 6 2002

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Data File C:\HPCHEM\l\DATA\02MAR06\05161.D Vial: 14 Acq On 7 Mar 2002 1:18 am Operator: 201-wb Sample nyc Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP022702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L

Peak Number 1 Hydrazine, 1,2-diethyl- Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 15.73 0.03 ug/L 19705 1,4-DIFLUOROBENZENE 15.09 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Hydrazine, 1,2-diethyl- 88 C4H12N2 001615-80-1 4 2 1,3-Dioxolan-2-one 88 C3H403 000096-49-1 4 3 1,2 -Hydrazinedicarboxaldehyde 88 C2H4N2021 000628-36-4 4 4 3-Hexanone, 2-methyl- 114 C7H140 ______ 007379-12-6 4 Abundance Scan 690 (15.733 min): 05161 .D (-) m/z 114.15 100.00% 1 4

5000 63 ' ■ i ■ '' ■ i • ■ ■ i' ■ ■ ■ i 88 15.40 15.60 15.80 16.00 44 m/z 63.05 29.30% m/z-> • i ■ ■ • • i ■

10 20 11 ■ ■ ■ ■ i ■ ■ ■ ‘ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■1 ■ ■ i ■

30 40 50 60 70 80 ..I90.......... 100 110 120 TT-p-t

Abundance #840: Hydrazine, 1,2-diethyl- 31 59 88

5000 44 73 15.40 15.60 15.80 16.00 m/z 88.00 23.62%

— i T-p-n-r-p-T 1" " l‘" " I ■' i ■' ■111 ■ ■ ■ i ■ ■ ■ ■ i ■ ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #62892: 1,3-Dioxolan-2-one 29

15.40 15.60 15.80 16.00 5000 43 m/z 43.95 14.44% 88 WAWWy 58 ‘ i • ■ ■ ■ i ■ ■ ■ ■ I ■ TIH+ । • 11 > • ■ • । ■ i • • I ‘ ‘ ‘ I ‘ ' I ' ' ' ' I ' 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #781: 1,2-Hydrazinedicarboxaldehyde 31 15.40 15.60 15.80 16.00

60 88 5000

44 17 ...... | — T-pm-p-TT ’*I*’*’+* I' ' ‘ ' i • ■ ‘ ‘ l' ‘ ' 11 ‘ 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120

05161.D HP022702.M Thu Mar 07 09:02:50 2002 Page 1

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