Volatile organic compounds results, Mar 6 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\l\DATA\02MAR06\05156.D Vial: 9 Acq On 6 Mar 2002 7:31 pm Operator: 201-wb Sample nyc Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP022702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L Peak Number 1 1-(Propenylthio)prop-l-ene Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 15.75 0.03 ug/L 19528 1,4-DIFLUOROBENZENE 15.09 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-(Propenylthio)prop-l-ene 114 C6H10S 000000-00-0 3 2 2,4-Imidazolidinedione, 3-methyl- 114 C4H6N2O2! 006843-45-4 3 3 3-Cyclobutene-l,2-dione, 3,4-dihydr 114 C4H2O4 002892-51-5 2 4 2-Pentenoic acid, methyl ester 114 C6H10O2 ______ 000818-59-7 2 Abundance Scan 692 (15.750 min): 05156.D (-) m/z 114.05 100.00% 1 4

8000

6000 | — 4000 1 1 I' 1 1 1 I ' 15.40 15.60 15.80 16.00 63 88 m/z 88.10 22.85% i ■ ■ ‘ ■ i ■ ■ ■ ■ i ■ ■ ■ ‘ i ■ ■ ■ ■ i ■ ' ' ■ i ■ ■ ■ ■ i ■ • ■ 1 i ■ ' ■ ■ i ■ ■ ' ■ i ‘ m/z--> 20 30 40 50 60 70 80 90 100 110 120 / Abundance #2940:1-(Propenylthio)prop-1-ene 1 14 41 99

5000 15.40 15.60 15.80 16.00 m/z 63.05 21.25% cq 73 85 i ‘ ' i ‘ ‘ ■ । । • ■ ■ । • ■ ■ ■ । ■ ■ ■ i ' ' • • i ■ ■ ■ ■ । I ' 1 1 1 I ' • >i■ < /z—> 20 30 40 50 60 70 80 90 100 110 120 Abundance #64088:2,4-Imidazolidinedione, 3-methyl- 1 14

• i »»• ■ i ■ T1 15.40 15.60 15.80 16.00 58 5000

86

42 71 ri ■ ■ 1 ■ i ■ • ■ ■ i ‘ ‘ i ■ ■ ■ ■ i ■ ■ • ■ i ■ ‘ ■ i ■ ■ ■ i ■ ■ ■ • i ■ ‘ • i ■ ‘ 14* n/z—> 20 30 40 50 60 70 80 90 100 110 120 Abundance #64087:3-Cyclobutene-1,2-dione, 3,4-dihydroxy- 29 58

5000 114

m/z-> 20 l 30 40 50 ’1’ 68____ 86 60 _______ -n-p-r 11*11*111111*111122911213 70 80 90 100 110 120

05156.D HP022702.M Thu Mar 07 08:55:21 2002 Page 1

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