Volatile organic compounds results, Mar 4 2002

NYC 9/11 Public Portal Document Llprary searcn compound Report Data File C:\HPCHEM\l\DATA\02MAR04\04377.D Vial: 11 Acq On 4 Mar 2002 5:26 pm Operator: 201-wb Sample nyc Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP022702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L Peak Number 2 Ethanamine, N-methyl-N-nitroso Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 15.77 0.03 ug/L 20957 1,4-DIFLUOROBENZENE 15.10 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Ethanamine, N-methyl-N-nitroso- 88 C3H8N20 010595-95-6 3 2 1,2-Hydrazinedicarboxaldehyde 88 C2H4N202! 000628-36-4 3 3 1,4-Dioxane 88 C4H802 000123-91-1 3 4 Propane, 1-ethoxy- 88 C5H120 ______ 000628-32-0 3 Abundance Scan 692 (15.766 min): 04377.D (-) m/z 114.15 100.00% 1 4

5000

63 88 1. 15.40 15.60 15.80 16.00 ___ ______________ 44__________________ m/z 88.10 23.78% ' ' i1 ■ ■ ■ i ■ ■' ■ i' ‘ ‘ ' I ' ‘ ■ i ■ ' ‘ ‘ i ■ '' ‘ i ■ ‘ ‘' i' ' 1111' 11'1' 11 1 ■ i ■1 / m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #62895: Ethanamine, N-methyl-N-nitroso- 42 88

5000 15.40 15.60 15.80 16.00 56 m/z 62.95 21.54% 73

m/Z-> E1’ 10 20 30 40 LU 50 TTT 1111:1111*117111111 60 70 80 90 100 110 120 ' i ‘ 1 ' i ■

Abundance #62891:1,2-Hydrazinedicarboxaldehyde 31 ■ i ‘1 ' ■ i ■ ■ • i * * * • i * ' ' ' । * 15.40 15.60 15.80 16.00 5000 m/z 44.00 3.89%

16 45 60 88 ’WwyM m/z-> H 10 20 — 30 40 50 60 70 80 90 100 110 120 1' i' • ■ ■ i ‘ ‘ i' ' ■ ‘ i ‘ ' ■ i ‘ ■ ■ ■ i ' ‘

Abundance #794: 1,4-Dioxane 29 88 15.40 15.60 15.80 16.00

58

5000 15

45

m/z--> - 10 20 —H 30 40 50 60 70 80 i ■ ■ ■ ■ i ‘ ■ ■ ■ i • ■ 90 100 110 120

04377.D HP022702.M Tue Mar 05 08:42:09 2002 Page 2

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