Volatile organic compounds blank results, Mar 8 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\O2MARO8\5174.D Vial: 11 Acq On 8 Mar 2002 6:21 pm Operator: 201-wb Sample nyc Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP022702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Ethanamine, N-methyl-N-nitroso Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 15.70 0.03 ug/L 18508 1,4-DIFLUOROBENZENE 15.05 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Ethanamine, N-methyl-N-nitroso- 88 C3H8N20 010595-95-6 3 2 1,2-Hydrazinedicarboxaldehyde 88 C2H4N202’ 000628-36-4 3 3 1,4-Dioxane 88 C4H802 000123-91-1 3 4 Propane, 1-ethoxy- 88 C5H120 ______ 000628-32-0 3 Abundance Scan 689 (15.699 min): 5174.D (-) m/z 114.15 100.00% 1 4

5000 63 88 15.40 15.60 15.80 16.00 44 1’111 m/z 63.05 27.51% ■ ■ i ■ ■ ■ ‘ i ■ ‘‘ i' ' ‘ ■ i ' ‘ ' i ■ ■ ‘ ‘ i ‘ ‘ i ‘ ‘ ‘ ‘ i ‘ ‘ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #62895: Ethanamine, N-methyl-N-nitroso- 42 88

5000 15.40 15.60 15.80 16.00 m/z 88.00 25.34% 56

m/z-> ’•I14+’I’’’’I+**’)* 10 20 30 40 LX 50 60 70 73 1 80 i ■ ■ ■ ‘ i ■ • ■ ■ i ■ ' ■ ■ i ■ ■ 90 100 110 120 Abundance #62891:1,2-Hydrazinedicarboxaldehyde 31 ■ ■ i ■ 1 ■ ‘ i ■ 1' i1 ' ‘ ‘ i'' 15.40 15.60 15.80 16.00 5000 m/z 43.95 4.17% 60 88 WWWWy” m/z-> 4 —l,H 10 16

20 30 40 45 50 60 ■11 ■1111 ■ ■ 70 80 i ■ ‘ ■11 ■ ■ ■ ■ i ‘1 ■ ■ i ■1 90 100 110 120 Abundance #794: 1,4-Dioxane 29 88 15.40 15.60 15.80 16.00

58

5000 15

m/z--> - 10 20 30 ,115, H i ■ ■ ■' i''' ■ i ■ ■ 40 50 60 70 80 90 100 110 120 i ■ ■'' i ■ ■ ‘ ■ i ■'1' i' ■

5174.D HP022702.M Sun Mar 10 13:09:09 2002 Page 2

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