VOC analysis results, sample AE03934, Feb 27 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\02FEB27\0227C10B.D Vial: 21 Acq On : 28 Feb 2002 1:06 am Operator: Sample : cal 10 Inst : 210 Mise : February 27, 2002 Multiplr: 1.00 MS Integration Params: GAS5.P Quant Time: Feb 28 8:11 2002 Quant Results File: HP021102.RES

Quant Method : C:\HPCHEM\1\METHODS\HP021102.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Thu Feb 28 08:10:08 2002 Response via : Initial Calibration DataAcq Meth : HP021102

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-DIFLUOROBENZENE 15.58 114 1043029 5.00 ug/L 0.00 21) CHLOROBENZENE-D5 23.34 82 547547 5.00 ug/L 0.00 49) 1,4-DICHLOROBENZENE-D4 29.39 152 471278 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,2-Dichloroethane-d4 14.63 65 243973 5.51 ug/L 0.00 Spiked Amount 5.000 Recovery = 110.20% 22) Toluene-d8 19.49 98 1321704 4.77 ug/L 0.00 Spiked Amount 5.000 Recovery = 95.40% 50) 4-Bromofluorobenzene 26.39 95 492938 5.01 ug/L 0.00 Spiked Amount 5.000 Recovery = 100.20%

Target Compounds Qvalue 3) DICHLORODIFLUOROMETHANE 4.22 85 739845 10.79 ug/L 98 4) CHLOROMETHANE 4.83 50 809646 13.73 ug/L 96 5) VINYL CHLORIDE 4.89 62 1055529 14.43 ug/L 100 6) BROMOMETHANE 5.74 96 506569 10.63 ug/L 98 7) CHLOROETHANE 5.88 64 674261 14.60 ug/L 98 8) TRICHLOROFLUOROMETHANE 6.41 101 760942m 11.08 ug/L 9) ACETONE 8.08 43 8493 7.19 ug/L 97 10) 1,1-DICHLOROETHENE 7.79 61 925738 9.54 ug/L 91 11) METHYLENE CHLORIDE 8.98 49 924898 10.21 ug/L 95 12) METHYL TERT BUTYL ETHER 9.29 73 1268782 10.36 ug/L 98 13) TRANS-1,2-DICHLOROETHENE 9.73 61 1051300 10.61 ug/L 94 14) 1,1-DICHLOROETHANE 10.82 63 1348696 11.21 ug/L 100 15) 2-BUTANONE (MEK) 12.22 43 68815 15.69 ug/L 93 16) 2,2-DICHLOROPROPANE 12.26 77 868170 9.88 ug/L 98 17) CIS-1,2-DICHLOROETHENE 12.40 61 1075076 11.41 ug/L 94 18) CHLOROFORM 12.79 83 1297527 11.26 ug/L 98 19) BROMOCHLOROMETHANE 13.25 49 501553 11.46 ug/L 93 20) 1,2-DICHLOROETHANE 16.91 62 557988 11.25 ug/L 98 23) 1,1,1-TRICHLOROETHANE 13.82 97 1026904 10.99 ug/L 100 24) 1,1-DICHLOROPROPENE 14.24 75 1068383 10.77 ug/L 98 25) CARBON TETRACHLORIDE 14.50 117 735306 10.63 ug/L 98 26) BENZENE 14.93 77 805188 9.89 ug/L 97 27) TRICHLOROETHENE 16.47 95 804345 10.44 ug/L 99 28) 1,2-DICHLOROPROPANE 16.91 63 779046 10.51 ug/L 99 29) DIBROMOMETHANE 17.67 174 240249 10.16 ug/L 94 30) BROMODICHLOROMETHANE 17.51 83 781255 10.37 ug/L 99 31) 2-CHLOROETHYL VINYL ETHER 19.69 63 286026 11.41 ug/L 91

(#) = qualifier out of range (m) = manual integration 0227C10B.D HP021102.M Thu Feb 28 08:11:32 2002 Page 1

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