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VOC analysis results, sample AE03944, Feb 20 2002

Machine-extracted title · confidence 95%

Laboratory results for volatile organic compounds in sample AE03944 analyzed on February 20, 2002.

NYC-WTC_000020143–000020240

Folder label: “524 2/20/02

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Scanned page image, NYC-WTC_000020233
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\02FEB20\03952.D Vial: 17 Acq On : 20 Feb 2002 9:14 pm Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise : February 20, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP021702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L

Peak Number 1 Acetonitrile, dichloro- Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 17.30 0.02 ug/L 23820 1,4-DIFLUOROBENZENE 15.15 Hit# of 5 Tentative ID MW MolForm CAS# Qual

l Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 28 2 Acetic acid, hydrazide 74 C2H6N20 001068-57-1 3 3 Carbon dioxide 44 CO2 000124-38-9 2 4 Nitrous Oxide 44 N20 _______ 010024-97-2 2 Abundance Scan 783 (17.298 min): 03952.D (-) m/z 73.95 100.00% 74 8000

6000 82

47 4000 17.00 17.20 17.40 17.60 IEBEOUIEESUUUETIETT Th ‘ r■ ■ ‘i"''i m/z 82.00 58.24% m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #63810: Acetonitrile, dichloro- 74 35

5000 82 17.00 17.20 17.40 17.60 47 m/z 46.95 40.64% 39

m/z-> T Tnmaugt T TTTp- 1186• * J' * ’ * J 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #307: Acetic acid, hydrazide 43 17.00 17.20 17.40 17.60 31 m/z 84.00 34.89% 5000 15

27

m/z-> 'I........ ...... "i" "i" mHr " "I ■'' ■ I 'I' ■ I "■ I"''

5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 I 59 "I I H ' 1111" I' n 11 ii । 74 1111111II U| n 11111 u | ii 111

Abundance #62263: Carbon dioxide 44 17.00 17.20 17.40 17.60 m/z 76.00 28.05% / 5000

1216 _ • "j'l"!' 1 1..................... j 22 "■ i ■■ ■ ■! ■ ■■ ■ r ,T'111" 11''11" " II'1 p' | ' 111 "I | 11111" । ii ii ii

m/z--> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 17.00 17.20 17.40 17.60

03952.D HP022702.M Mon Mar 04 17:31:17 2002 Page 1

NYC-WTC_000020233

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NYC-WTC_000020233Source: NYC Law Department, mirrored locally

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