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VOC analysis results, sample AE03947, Feb 22 2002

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Laboratory results for volatile organic compounds in sample AE03947 analyzed on February 22, 2002.

NYC-WTC_000020242–000020383

Folder label: “524 2/21/02 - 2/22/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\02FEB21\3947D.D Vial: 10 Acq On : 22 Feb 2002 3:05 am Operator: 201-wb Sample : nyc; dup Inst : GC/MS Ins Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP021702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Acetonitrile, dichloro- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 17.28 0.05 ug/L 73502 1,4-DIFLUOROBENZENE 15.14 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 12 2 Hydrazinecarboximidamide 74 CH6N4 000079-17-4 4 3 Propanoic acid 74 C3H602 000079-09-4 4 4 N-Nitrosodimethylamine 74 C2H6N20 ________ 000062-75-9 3 Abundance Scan 781 (17.282 min): 3947D.D (-) m/z 73.95 100.00% 7(4

82

5000 47

17.00 17.20 17.40 17.60

m/z-> . ............. A311,.., 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 ........ |... Tn-fT m/z 82.00 71.14%

Abundance #63810: Acetonitrile, dichloro- 74

35

5000 82 17.00 17.20 17.40 17.60 47 m/z 76.00 47.25% 39 mth t....j।1 TTTfT 86 TPUpuu m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #303: Hydrazinecarboximidamide 74 43 17.00 17.20 17.40 17.60 5000 m/z 84.00 44.27% 30 57 17

/z-> ---------- “r"‘r ’’’’I’N 1163.. . T 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #322: Propanoic acid 29 74 17.00 17.20 17.40 17.60 m/z 47.05 43.37% 45

5000 57

TmpgT —374Hm TrfTTrrp-rrrpT J....।.. 1.14..411.11j TITIfIfPmmamof /z--> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 17.00 17.20 17.40 17.60

3947D.D HP021702.M Mon Feb 25 12:12:23 2002 Page 5

NYC-WTC_000020383

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NYC-WTC_000020383Source: NYC Law Department, mirrored locally

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