VOC analysis results, sample AE03958, Feb 19 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\02FEB19\03958.D Vial: 5 Acq On : 19 Feb 2002 8:47 pm Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise : February 19, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP021702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L

Peak Number 1 Glycinamide hydrochloride Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 17.23 0.02 ug/L 16752 1,4-DIFLUOROBENZENE 15.09 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Glycinamide hydrochloride 74 C2H6N20 001668-10-6 4 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 4 3 Acetic acid, hydrazide 74 C2H6N20 001068-57-1 3 4 Nitrous Oxide 44 N20 ______ 010024-97-2 2 Abundance Scan 778 (17.231 min): 03958.D (-) m/z 73.95 100.00% 74 82 5000 47 ■ ■ i ■ • • ■ i ■ ■ ' i ■ ■ ■ ■ i ■ ■ 17.00 17.20 17.40 17.60 r।।.... ।.... । TUU— m/z 82.00 60.63% m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 N Abundance #306: Glycinamide hydrochloride 44

74 5000 ■ ■ i ■ ■ TT-p-n-r-p-r 17.00 17.20 17.40 17.60 57 m/z 46.95 41.41%

pTTTpTTTpTTTprTTpTrrpTT^^ frpm pmpmpm m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #63810: Acetonitrile, dichloro- 74 35 f 17.00 17.20 17.40 17.60 5000 82 m/z 76.00 31.64%

47 39 B’EU-—EIIUTCEUOEOITTEIETTT AltTTTpp T TTT]T 86 i ■ • “i ■ ■ ■ 'i m/z--> i5 10 15 20 25 3035404550556065 70 75 808590 Abundance> #307: Acetic acid, hydrazide 43 17.00 17.20 17.40 17.60 m/z 43.95 4.70% 31 WAW/M 5000 15

। 59 74 i“"ru "IEETETTB""I——B—B—UETI’ET7T m/z-> 5 10 15 20 25 3035404550556065 70 75 808590 17.00 17.20 17.40 17.60

03958.D HP021702.M Mon Mar 04 10:46:24 2002 Page 1

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