Volatile organic compounds blank results, Feb 28 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\02FEB27\3917.D Vial: 3 Acq On : 27 Feb 2002 6:49 pm Operator: 201-wb Sample : nyc 524 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP022702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L

Peak Number 3 Acetonitrile, dichloro­ Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 17.32 0.06 ug/L 113926 1,4-DIFLUOROBENZENE 15.17 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 37 2 Thiirane, methyl- 74 C3H6S 001072-43-1 7 3 Glycinamide hydrochloride 74 C2H6N20 001668-10-6 5 4 Ether 74 C4H10O ______ 000060-29-7 4 Abundance Scan 784 (17.316 min): 3917.D (-) m/z 73.95 100.00% 74 82

5000 47 ......... /.A... 17.00 17.20 17.40 17.60

m/z-> F2,,55. " ■i■■ “ i■■■ • i ■ • ‘ 'i 1 111 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Tn-p- I'1 " I ‘ 'I m/z 82.00 71.47%

Abundance #63810: Acetonitrile, dichloro- 74 35

5000 82 • t • ■ ' ■ i ■ ■ ■ ■ i 17.00 17.20 17.40 17.60 88 47 m/z 84.00 41.23%

TTTT —mmmmmppt " ' I ' 86 m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #324: Thiirane, methyl- 41 74

17.00 17.20 17.40 17.60 45 m/z 46.95 37.59% 5000 59 27 37 .. JLu mph ...life.. ...11... “I” m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #306: Glycinamide hydrochloride ----- 44 17.00 17.20 17.40 17.60 m/z 76.10 32.48% 74 5000

41 57

m/z-> ■ ■ • | |■■■'! “ ■ . . ■. | 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 7 TTT “ “ I ‘ ‘' 'I “ “ i'11 'I 17.00 17.20 17.40 17.60

3917.D HP022702.M Thu Mar 07 17:20:47 2002 Page 3

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