VOC analysis results, sample AE03958, Feb 19 2002

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Data File : C:\HPCHEM\1\DATA\02FEB19\03802F.D Vial: 17 Acq On : 20 Feb 2002 5:26 am Operator: 201-wb Sample : nyc fb Inst : GC/MS Ins Mise : February 19, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP021702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Urea, N,N-dimethyl- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. 15.77 0.04 ug/L 31694 1,4-DIFLUOROBENZENE 15.10 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Urea, N,N-dimethyl- 88 C3H8N20 000598-94-7 5 2 Urea, ethyl- 88 C3H8N20 000625-52-5 4 3 Ethanedial, dioxime 88 C2H4N202! 000557-30-2 4 4 2,3-Dioxabicyclo[2.2.2]octane 114 C6H10O2 ________ 000000-00-0 4 Abundance Scan 693 (15.766 min): 03802F.D (-) m/z 114.15 100.00% 14

5000

63 88 50 15.40 15.60 15.80 16.00 • ■ i ■ ‘ m/z 88.00 23.37% ■' i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ‘ i' ■ ■ ■ i ■ ■ ■ ■ i' ■ ■ ■ i'' i • ■ ■ ■ i ■ ■ ■ ■ i ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #62896: Urea, N,N-dimethyl- 44

5000 88 ■ i ■ ■ ■ ■ i ■ ■ T-ry-r-n-r-p- 15.40 15.60 15.80 16.00 m/z 63.05 23.25% 15 72 /z-> TIIrt 10 20 1 30 40 56 ‘ ‘ I''' ■ I ■ ''' 11 ‘

50 60 70 80 ‘ 1' ‘ 90 100 110 120 Abundance #789: Urea, ethyl- 33 44 73 ■ i * • 1 1 i * ■ ’11’44’11 88 15.40 15.60 15.80 16.00 5000 m/z 57.05 15.95% N 56

m/z-> 10 .... V ..,1 , '' 20 30 i 40 Ipfm,.. 90 100 110 120 50 60 70 80 Abundance #783: Ethanedial, dioxime 44 15.40 15.60 15.80 16.00 16 m/z 50.05 15.41% 27 88 70 5000 53

■ < । > TTT 1 ■ i ■ •'11 ■ i

m/z--> 10 20 30 40 50 60 70 80 90 100 110 120 15.40 15.60 15.80 16.00

03802F.D HP022702.M Mon Mar 04 12:18:31 2002 Page 1

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