VOC analysis results, sample AE03015, Feb 15 2002

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Data File : C:\HPCHEM\1\DATA\02FEB15\03381F.D Vial: 34 Acq On : 16 Feb 2002 12:03 pm Operator: 201-wb Sample : nyc fb Inst : GC/MS Ins Mise : February 15, 2002 Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Method : C:\HPCHEM\1\METHODS\HP021302.M (RTE Integrator) Title : VOCS BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L Peak Number 1 Urea, ethyl- Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 15.81 0.03 ug/L 30615 1,4-DIFLUOROBENZENE 15.15 Hit# of 5 Tentative ID MW MolForm CAS# Qual l Urea, ethyl- 88 C3H8N20 000625-52-5 4 2 1-(Propenylthio)prop-l-ene 114 C6H10S 000000-00-0 3 3 1,4-Butanediamine 88 C4H12N2 000110-60-1 3 4 3-Butenoic acid, ethyl ester 114 C6H10O2 ______ 001617-18-1 3 Abundance Scan 685 (15.809 min): 03381 F.D (-) m/z 114.15 100.00% 1' 4

5000 63 88 w. }**’*i’* TT-p-T 15.40 15.60 15.80 16.00 16.20 ............................... 44 ............................... m/z 63.05 22.81% m/z-> Abundance 10 20 30

33 40

44 50 60 70 80 #789: Urea, ethyl- I 1 ' ‘ ' I ‘ ' 1 ' I 1 90 100 110 120 1 ‘ I ' 1

A 73 88 5000 i ■ ‘ ■ 11' mseoug 15.40 15.60 15.80 16.00 16.20 m/z 88.10 22.17%

m/z--> -77 10 20 30 40 L 90 100 110 120 ■ ■ i 50 56

60 70 80 i ■ ■ ■ ■ i ■ ■ ■ ■ i'' ■ ■ i' ■

Abundance #2940: 1-(Propenylthio)prop-1-ene 1 4 41 99 ■ ' i ■ 1 1 11 ■1 15.40 15.60 15.80 16.00 16.20 5000 m/z 43.95 2.65% M-NAAMMM 59 73 85 ■ i ■ ■ ■ ■ i • ■ ■ ■ i ■ ‘ ■ i ■ ■1 ‘ 11 " I' ■' ■ I " " I ■. " I' -rrp-r m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #828:1,4-Butanediamine 33 15.40 15.60 15.80 16.00 16.20

5000 43

n/z-> • i • ■ > • i ■ > 10 20 30 L , 40 , 50 59 60 70 88 ■ ■ I’1 ■ ■ ■ i ■ ■ ■11 ■ ■ ■ ■ i ■ ■ ■ ■ ।

70 80 90 100 110 120 ■ i ‘ ■

03381F.D HP021302.M Mon Feb 18 15:36:55 2002 Page 1

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